Fracture-hole type water-driven flexible flow regulating particle and preparation method thereof
A water-flooding flexible, fracture-cavity technology, applied in chemical instruments and methods, drilling compositions, etc., to achieve the effects of low cost, adjustable strength, and long stability period
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[0039] According to another aspect of the present invention, the present invention provides a method for preparing fracture-cavity water-flooding flexible flow-regulating particles, comprising the following steps:
[0040] (1) After stirring the clear water and the clay evenly, add N-vinylpyrrolidone and acrylamide, stir evenly, and let stand;
[0041] In a preferred embodiment, step (1) is: add clay solution and clear water into the mixing tank, stir until the solution is dispersed and stable, then add N-vinylpyrrolidone and acrylamide and stir evenly, and leave the above solution for 3 Hour;
[0042] The above solution was left to stand for 3 hours in order to better gel.
[0043] The salinity of the above-mentioned clear water is lower than 1000 mg / L, and the clear water can be tap water.
[0044] (2) Add N, N-dimethylene bisacrylamide solution, after stirring evenly, add sodium formaldehyde sulfoxylate and ammonium persulfate solution;
[0045] Wherein, N, N-dimethylene...
Embodiment 1
[0054] Add 4 parts by weight of sodium bentonite in clear water and stir evenly, then add 20 parts by weight of N-vinylpyrrolidone and 40 parts by weight of acrylamide and stir evenly, let stand; add 0.5 parts by weight of N,N-di After stirring the solution of methylenebisacrylamide evenly, a solution containing 0.5 parts by weight of sodium formaldehyde sulfoxylate and 0.3 parts by weight of ammonium persulfate was added to the mixture, stirred; nitrogen gas was introduced for 35 minutes, and heated to After 3 hours at 50°C, it was sheared by a colloid mill to obtain fracture-cavity water flooding flexible flow-regulating particles with a particle size of 2-5 mm, wherein the total content of clean water used was 34.7 parts by weight.
Embodiment 2-7
[0056] The fracture-cavity water flooding flexible flow-regulating particles were prepared according to the same steps as in Example 1, and the technical parameters of each example are shown in the table below.
[0057] Summary of technical parameters of Table 1 Embodiment 2-7
[0058]
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