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Efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material and method for preparing same

A technology of glass fiber cloth and photocatalytic materials, which is applied in chemical instruments and methods, separation methods, physical/chemical process catalysts, etc., can solve the problems of waste, catalytic activity needs to be improved, and cannot be effectively separated and recycled, and the reaction conditions can be met. Mild and easy to control, good catalytic activity and stability, and uniform catalyst distribution

Active Publication Date: 2018-09-14
HUAZHONG NORMAL UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the catalyst bismuth oxychloride used in the catalytic reaction process usually exists in the form of powder. On the one hand, it cannot be separated and recovered effectively, which is easy to cause waste. On the other hand, its catalytic activity needs to be improved.

Method used

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  • Efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material and method for preparing same
  • Efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material and method for preparing same
  • Efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material and method for preparing same

Examples

Experimental program
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Effect test

Embodiment 1

[0030] To prepare a kind of glass fiber cloth with high efficiency for degrading NO in situ loaded BiOCl photocatalytic material, the specific steps are as follows:

[0031] Step 1, soak the glass fiber cloth with 3% hydrofluoric acid for 60 minutes;

[0032] Step 2, wash the glass fiber cloth twice with deionized water and ethanol respectively, and then dry it;

[0033] Step 3, adding 7 mmol of bismuth nitrate pentahydrate into deionized water to form a 1L solution, and stirring until the bismuth nitrate pentahydrate no longer dissolves;

[0034] Step 4. Add 7 mmol potassium chloride into deionized water, stir until the potassium chloride is completely dissolved, and make a 1L solution;

[0035] Step 5, soak the glass fiber cloth obtained in step 1 in the solution prepared in step 2, take it out after 10 seconds, put it on filter paper to absorb the surface solution;

[0036] Step 6. Soak the glass fiber cloth used to absorb the surface solution in step 4 in the solution pr...

Embodiment 2

[0047] To prepare a kind of glass fiber cloth with high efficiency for degrading NO in situ loaded BiOCl photocatalytic material, the specific steps are as follows:

[0048] Step 1, soak the glass fiber cloth with a 4% hydrofluoric acid solution for 30 minutes;

[0049]Step 2, wash the glass fiber cloth twice with deionized water and ethanol respectively, and then dry it;

[0050] Step 3, adding 5 mmol of bismuth nitrate pentahydrate into deionized water to form a 1L solution, and stirring until the bismuth nitrate pentahydrate no longer dissolves;

[0051] Step 4. Add 5 mmol potassium chloride into deionized water, stir until the potassium chloride is completely dissolved, and make a 1L solution;

[0052] Step 5, soak the glass fiber cloth obtained in step 2 in the solution prepared in step 3, take it out after 20 seconds and put it on filter paper to absorb the surface solution;

[0053] Step 6. Soak the glass fiber cloth used to absorb the surface solution in step 4 in th...

Embodiment 3

[0058] To prepare a kind of glass fiber cloth with high efficiency for degrading NO in situ loaded BiOCl photocatalytic material, the specific steps are as follows:

[0059] Step 1, soak the glass fiber cloth with a 5% hydrofluoric acid solution for 20 minutes;

[0060] Step 2, wash the glass fiber cloth twice with deionized water and ethanol respectively, and then dry it;

[0061] Step 3, adding 10 mmol of bismuth nitrate pentahydrate into deionized water to form a 1L solution, and stirring until the bismuth nitrate pentahydrate no longer dissolves;

[0062] Step 4, add 10mmol potassium chloride into deionized water, stir until the potassium chloride is completely dissolved, and make a 1L solution;

[0063] Step 5, soak the glass fiber cloth obtained in step 1 in the solution prepared in step 2, take it out after 10 seconds and put it on filter paper to absorb the surface solution;

[0064] Step 6. Soak the glass fiber cloth used to absorb the surface solution in step 4 in ...

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Abstract

The invention relates to an efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material. The efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalyticmaterial comprises glass fiber cloth and BiOCl layers. The BiOCl layers grow on the glass fiber cloth in an in-situ manner, and BiOCl nano-sheets are densely assembled to obtain the BiOCl layers. A method for preparing the efficient NO degradation glass fiber cloth in-situ loaded BiOCl photocatalytic material includes 1), soaking the glass fiber cloth in hydrofluoric acid solution and then washingand drying the glass fiber cloth for standby application; 2), soaking the glass fiber cloth in saturated solution of bismuth nitrate pentahydrate, then taking the glass fiber cloth out of the saturated solution and draining solution attached to the surfaces of the glass fiber cloth; 3), soaking the glass fiber cloth obtained at the step 2) in potassium chloride solution, then taking the glass fiber cloth out of the potassium chloride solution and draining solution attached to the surfaces of the glass fiber cloth; 4), repeatedly carrying out the step 2) and the step 3) and ultimately drying the glass fiber cloth to obtain the BiOCl photocatalytic material on the basis of the glass fiber cloth.

Description

technical field [0001] The invention belongs to the technical field of inorganic materials, and in particular relates to a BiOCl photocatalytic material based on glass fiber cloth and a preparation method thereof. Background technique [0002] Bismuth oxychloride is an inorganic material, mostly used in the pigment market. Recently, bismuth oxychloride as a new type of photocatalyst has attracted widespread attention. Previous studies have shown that bismuth oxychloride has better photocatalytic activity than commercial titanium dioxide P25 and other catalysts under full light irradiation. Chinese patent CN101879455B provides a photocatalyst, bismuth oxychloride, which is used for photocatalytic oxidation of organic matter in water. The research results show that the bismuth oxychloride photocatalyst has good photocatalytic activity, and can be used in sunlight and simulated sunlight. The effect is comparable to that of the commercialized P25 photocatalyst; under the irrad...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J27/06B01J35/06B01D53/86B01D53/56
CPCB01D53/8628B01J27/06B01D2255/802B01J35/30B01J35/23B01J35/58B01J35/39Y02C20/30
Inventor 艾智慧龚旭阳张礼知严义清严方升
Owner HUAZHONG NORMAL UNIV
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