A kind of continuous extraction method of pepper oleoresin
An extraction method and technology of pepper oil, which is applied in the field of continuous extraction of pepper oleoresin, can solve the problems of long solvent concentration process, loss of heat-sensitive active ingredients, and influence on product flavor, etc., and achieve large-scale industrial production and reduce the amount of extraction solvent Less, reduced loss effect
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Embodiment 1
[0036]Step 1: Preparation of raw materials: 1000kg of black pepper powder with a piperine content of 8.1% was extracted, the crushed pepper was subjected to extraction of essential oil, and the essential oil was extracted by continuous steam distillation. The essential oil in the pepper is first extracted, which can avoid the large loss of volatile essential oil caused by the concentration and desolventization process of the essential oil and pepper oleoresin in the one-step extraction.
[0037] Step 2: Pretreatment: The pepper powder after extracting the essential oil is pretreated, and the pretreatment solution used is a mixed solution of propylene glycol, citric acid and water, wherein propylene glycol accounts for 79% of the mixed solution, and citric acid accounts for 1% of the mixed solution , the rest is pure water, the amount of the mixed solution used for pretreatment accounts for 0.5% of the pepper powder weight after extracting the essential oil, and the pretreatment...
Embodiment 2
[0042] Step 1: Preparation of raw materials: 2000kg of black pepper powder with a piperine content of 9.2% was extracted, the crushed pepper was subjected to extraction of essential oil, and the essential oil was extracted by continuous steam distillation. The essential oil in the pepper is first extracted, which can avoid the large loss of volatile essential oil caused by the concentration and desolventization process of the essential oil and pepper oleoresin in the one-step extraction.
[0043] Step 2: Pretreatment: The pepper powder after extracting the essential oil is pretreated, and the pretreatment solution used is a mixed solution of propylene glycol, citric acid and water, wherein propylene glycol accounts for 58% of the mixed solution, and citric acid accounts for 2% of the mixed solution , the rest is pure water, the consumption of the mixed solution used for pretreatment accounts for 2% of the pepper powder weight after extracting the essential oil, and the pretreat...
Embodiment 3
[0048] Step 1: Preparation of raw materials: 3000kg of black pepper powder with a piperine content of 10.0% was extracted, and the crushed pepper was subjected to extraction of essential oil. The equipment used for extraction of essential oil was a steam distillation tank. The essential oil in the pepper is first extracted, which can avoid the large loss of volatile essential oil caused by the concentration and desolventization process of the essential oil and pepper oleoresin in the one-step extraction.
[0049] Step 2: Pretreatment: The pepper powder after extracting the essential oil is pretreated, and the pretreatment solution used is a mixed solution of propylene glycol, citric acid and water, wherein propylene glycol accounts for 68.5% of the mixed solution, and citric acid accounts for 1.5% of the mixed solution , the rest is pure water, the amount of the mixed solution used for pretreatment accounts for 1.2% of the pepper powder weight after extracting the essential oil...
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