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Soaking type screw plate fixed-bed reactor for gas-solid catalytic reaction

A technology of fixed bed reactor and fixed bed reaction, which is applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of low utilization rate of catalyst bed space, difficulty in large-scale equipment, poor heat transfer effect, etc., and achieve High production capacity, less fouling and clogging, less floor space and less investment

Active Publication Date: 2018-06-05
QINGDAO UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In order to solve the technical problems of the existing shell-and-tube fixed bed reactor with poor heat transfer effect on the shell side, low space utilization rate of the catalyst bed, and difficulty in enlarging the device, the present invention provides A homogeneous spiral-plate fixed-bed reactor for gas-solid phase contact catalytic reaction

Method used

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  • Soaking type screw plate fixed-bed reactor for gas-solid catalytic reaction
  • Soaking type screw plate fixed-bed reactor for gas-solid catalytic reaction
  • Soaking type screw plate fixed-bed reactor for gas-solid catalytic reaction

Examples

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Embodiment 1

[0030] 150,000 tons / year dimethyl oxalate (DMO) hydrogenation reactor

[0031] When the reactor of the present invention is used as a 150,000-ton / year DMO hydrogenation reactor, it needs 8 spiral plate reaction sections after calculation. The structure is shown in image 3 with Figure 4 . The heat exchange medium inlet 1 is arranged on the top side of the reactor, and the outlet 2 is arranged on the upper side of the reactor. The gas enters the reactor from the top inlet 3, passes through the fixed catalyst bed (8-15), and then leaves the reactor with the product through the bottom gas outlet 4; the heat exchange medium passes through the annular tube distributor 5 at the top of the reactor. , Distributed by a number of distribution pipes 6 proportionally to the outer inlet of each spiral plate reaction section (08-15), heat exchange through the heat exchange medium channel spirally, enter the central tube 7 in the center of the reaction section, and then collect from the heat e...

Embodiment 2

[0037] 35,000 tons / year vinyl acetate synthesis reactor

[0038] When the reactor of the present invention is used as a 35,000-ton / year vinyl acetate synthesis reactor, it needs 10 spiral plate reaction sections after calculation. The structure is shown in Figure 5 with Image 6 . In order to further enhance the heat exchange effect, each spiral plate reaction section is equipped with a heat exchange medium to achieve segmented temperature control, specifically: heat exchange medium inlets 2,5-1 (medium temperature can be the same or different) are set at The lower part of the spiral plate reaction section is connected to the outside of the heat exchange medium channel inside the reaction section, and heat exchange through the heat exchange medium channel spirally enters the central tube 6-1 in the center of the reaction section and flows out from the heat exchange medium outlet 1. The gas enters the reactor from the top gas inlet 3, passes through the catalyst fixed bed (7-17)...

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Abstract

The invention relates to a soaking type screw plate fixed-bed reactor for a gas-solid catalytic reaction. The soaking type screw plate fixed-bed reactor comprises a gaseous phase and an inlet / outlet of a heat exchange medium; one or more screw plate fixed-bed reaction sections are arranged in the reactor. The soaking type screw plate fixed-bed reactor disclosed by the invention has the advantagesthat firstly, a shell pass heat exchange coefficient is remarkably increased, a total heat transfer coefficient is enabled to be increased, a heat transfer effect is intensified and heat transfer temperature difference is reduced; secondly, heat transfer distance and heat transfer area can be flexibly controlled and uniformity and control of the temperature of a reaction bed layer are facilitated;thirdly, the volume utilization rate is high (the maximum can reach 70 percent or higher, and the maximum of a shell and tube reactor is about 40 percent), the capacity of single equipment is high, and the occupied area and the investment are obviously reduced; fourthly, a heat exchange medium channel has a self-cleaning effect, so that dirt and block are not easily generated.

Description

Technical field [0001] The invention relates to a fixed bed reactor, in particular to a soaking type spiral plate fixed bed reactor for gas-solid catalytic reaction. Background technique [0002] Fixed-bed catalytic reactors are widely used in the chemical industry and petroleum industry. [0003] The advantages of the fixed-bed reactor are: ①The backmixing is small, the fluid can effectively contact the catalyst, and higher selectivity can be obtained when the reaction is accompanied by side reactions in series; ②The catalyst has low mechanical loss; ③Simple structure. The disadvantages are: ①The heat transfer effect in the shell side is poor, especially for strong exothermic reactions, which is prone to flying temperature (the reaction temperature is out of control, rises sharply, and exceeds the allowable range); ②The catalyst cannot be replaced during the operation and the catalyst needs to be regenerated frequently The reaction is generally not suitable for use, often replace...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/04
CPCB01J8/0465B01J8/0469B01J8/0496B01J2208/00132
Inventor 李建隆董纪鹏陈光辉范军领王伟文
Owner QINGDAO UNIV OF SCI & TECH
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