Soaking type screw plate fixed-bed reactor for gas-solid catalytic reaction
A technology of fixed bed reactor and fixed bed reaction, which is applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of low utilization rate of catalyst bed space, difficulty in large-scale equipment, poor heat transfer effect, etc., and achieve High production capacity, less fouling and clogging, less floor space and less investment
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Embodiment 1
[0030] 150,000 tons / year dimethyl oxalate (DMO) hydrogenation reactor
[0031] When the reactor of the present invention is used as a 150,000-ton / year DMO hydrogenation reactor, it needs 8 spiral plate reaction sections after calculation. The structure is shown in image 3 with Figure 4 . The heat exchange medium inlet 1 is arranged on the top side of the reactor, and the outlet 2 is arranged on the upper side of the reactor. The gas enters the reactor from the top inlet 3, passes through the fixed catalyst bed (8-15), and then leaves the reactor with the product through the bottom gas outlet 4; the heat exchange medium passes through the annular tube distributor 5 at the top of the reactor. , Distributed by a number of distribution pipes 6 proportionally to the outer inlet of each spiral plate reaction section (08-15), heat exchange through the heat exchange medium channel spirally, enter the central tube 7 in the center of the reaction section, and then collect from the heat e...
Embodiment 2
[0037] 35,000 tons / year vinyl acetate synthesis reactor
[0038] When the reactor of the present invention is used as a 35,000-ton / year vinyl acetate synthesis reactor, it needs 10 spiral plate reaction sections after calculation. The structure is shown in Figure 5 with Image 6 . In order to further enhance the heat exchange effect, each spiral plate reaction section is equipped with a heat exchange medium to achieve segmented temperature control, specifically: heat exchange medium inlets 2,5-1 (medium temperature can be the same or different) are set at The lower part of the spiral plate reaction section is connected to the outside of the heat exchange medium channel inside the reaction section, and heat exchange through the heat exchange medium channel spirally enters the central tube 6-1 in the center of the reaction section and flows out from the heat exchange medium outlet 1. The gas enters the reactor from the top gas inlet 3, passes through the catalyst fixed bed (7-17)...
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