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Low toxicity, low foam, and oil based slurry washing agent for well cementing and preparation method thereof

A flushing agent and oil-soaking technology, which is applied in the field of oil drilling and cementing, can solve the problems of water eutrophication, groundwater hazards, and affecting soil plant growth, etc., and achieve good flushing effect and good cementation effect

Active Publication Date: 2018-05-04
卫辉市化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Commonly used surfactants will kill microorganisms in the environment when they are discharged into the aquatic environment, inhibit the degradation of other toxic substances, and at the same time lead to a decrease in dissolved oxygen in the water, resulting in eutrophication of the water body; surfactants discharged into the soil will affect the growth of soil microorganisms. Effects on growth, thereby affecting soil plant growth and even potential harm to groundwater when migrating downwards

Method used

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  • Low toxicity, low foam, and oil based slurry washing agent for well cementing and preparation method thereof
  • Low toxicity, low foam, and oil based slurry washing agent for well cementing and preparation method thereof
  • Low toxicity, low foam, and oil based slurry washing agent for well cementing and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A low-toxic, low-foaming oil-based mud flushing agent for well cementing, consisting of the following raw materials (by weight): 65 parts of 5# white oil, 5 parts of soybean oil fatty acid, cardanol polyoxyethylene ether (HLB value 8 ) 10 parts, cardanol polyoxyethylene ether (HLB value 12) 10 parts and distilled water 10 parts.

[0023] The preparation method of the flushing agent is as follows: dissolving cardanol polyoxyethylene ether (HLB value 8) and cardanol polyoxyethylene ether (HLB value 12) in 5# white oil, then adding soybean oil fatty acid and distilled water and stirring Prepared evenly.

Embodiment 2

[0025] A low-toxic, low-foaming oil-based mud flushing agent for well cementing, consisting of the following raw materials (by weight): 55 parts of 5# white oil, 5 parts of soybean oil fatty acid, cardanol polyoxyethylene ether (HLB value 8 ) 10 parts, cardanol polyoxyethylene ether (HLB value 12) 10 parts and distilled water 15 parts.

[0026] The preparation method of described flushing agent is the same as embodiment 1.

Embodiment 3

[0028] A low-toxic, low-foaming oil-based mud flushing agent for well cementing, consisting of the following raw materials (by weight): 65 parts of 5# white oil, 10 parts of soybean oil fatty acid, cardanol polyoxyethylene ether (HLB value 8 ) 10 parts, cardanol polyoxyethylene ether (HLB value 12) 10 parts and distilled water 15 parts.

[0029] The preparation method of described flushing agent is the same as embodiment 1.

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Abstract

The invention discloses a low toxicity, low foam, and oil based slurry washing agent for well cementing. The slurry washing agent is mainly prepared from following raw materials in parts by weight: 45to 70 parts of basic oil, 5 to 10 parts of soybean oil fatty acid, and 20 to 30 parts of anacardol surfactant; wherein the anacardol surfactant comprises two anacardol surfactants with different HLBvalues: an anacardol surfactant with an HLB value of 8-9 and an anacardol surfactant with an HLB value of 10-12. The washing agent has a very good flushing effect on oil based slurry and mud cakes. The washing agent can be made into washing solutions with different concentrations and the foaming rate is extremely low. The experiment results show that when the addition amount of the washing agent is 20%, the foaming rate is less than 10%; the washing solution with 10 wt% of the washing agent has maximal washing efficiency close to 98%on a simulated borehole wall, and after washing, the direct cementing degree between the simulated borehole wall and cement paste is high.

Description

technical field [0001] The invention relates to the field of petroleum drilling and cementing, in particular to a low-toxic and low-foaming oil-based mud flushing agent for well cementing and a preparation method thereof. Background technique [0002] The flushing fluid belongs to the pre-cementing fluid, which is used before cementing, mainly for cleaning the oil stain on the well wall and gelling drilling fluid, improving the hydrophilic property of the cementing interface, and increasing the bonding strength between the interface and the cement sheath. And by improving the efficiency of cement slurry replacing drilling fluid, the purpose of improving cementing quality is achieved. [0003] Oil-based drilling fluid has good shale inhibition and excellent lubricity, and is widely used in shale gas wells, long horizontal well sections and other areas, and has achieved good drilling results. However, for well cementing, the oil film and oil-based mud cake formed by the oil-b...

Claims

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Application Information

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IPC IPC(8): C09K8/524
CPCC09K8/524
Inventor 穆莺梁艳丽卢甲晗张卫平张艺榉周嘉龙黄竟飞罗梓荣田婉君李新芬
Owner 卫辉市化工有限公司
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