Device and method for detecting dissolved oxygen in water
A technology for solubility and detection of water, which is applied in chemical analysis by titration, material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions, etc., which can solve unfavorable on-site operation and comparison. Reading error, slow speed and other problems, to achieve the effect of strong resistance to water quality interference, reduce error, and easy to carry
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Embodiment 1
[0041] Preparation of manganese sulfate solution: weigh 480gMnSO 4 4H 2 O, dissolved in distilled water, filtered and diluted to 1L.
[0042] Prepare alkaline KI solution: weigh 500g NaOH and dissolve in 300-400mL distilled water, weigh 150g KI and dissolve in 200mL distilled water, after the NaOH solution is cooled, combine the two solutions, mix well, and dilute to 1L with distilled water.
[0043] Fill bottle A1 with prepared MnSO in advance 4 1.0ml mixed with 2.0ml of alkaline KI solution, then vacuum decompressed and sealed, and bottle B2 was filled with concentrated H2 SO 4 2.0ml mixed with 1.0ml of 1% starch, then sealed under vacuum pressure reduction, bottle C3 filled with 100.0ml of 0.1mol / L NaS 2 o 3 solution. The amount of reagents and medicines in bottle A1 and bottle B2 is sufficient to react with water samples. Bottle A1 and bottle B2 are vacuum. The volume of bottle A1, bottle B2 and bottle C is 100ml, and the lower end of each bottle is an open slender ...
Embodiment 2
[0052] For ease of use, the elongated tubes at the bottom of the bottle A1, the bottle B2 and the bottle C3 can be made closed, and the bottle A1 and the bottle B2 are vacuum. The elongated tube is a glass tube with a pipe diameter of about 0.1mm, and the connecting branch of the four-way connecting pipe 5 is a flexible pipe. The elongated pipe can be tightly inserted into the connecting branch end of the four-way connecting pipe 5 .
[0053] During the detection process, when a reaction is required, the closed glass tube at the lower end of the bottle is broken directly, and the water sample can flow through the glass tube under the action of the pressure difference.
Embodiment 3
[0055] The slender tubes at the bottom of bottle A1, bottle B2 and bottle C3 are closed, and the slender cross-sections of the tubes are sealed with tinfoil, and bottle A1 and bottle B2 are in a vacuum state. Correspondingly, a thorn-shaped protrusion is provided on the inner side of the connecting hose of the four-way connecting pipe 5 . The elongated pipe can be tightly inserted into the connecting branch end of the four-way connecting pipe 5 .
[0056] During the detection process, when a reaction is required, bend the hose, use the thorn-shaped protrusion inside the hose to pierce the foil seal, and break the vacuum state, so that the water sample can flow through the glass tube under the action of the pressure difference.
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