Modified corncob adsorbent for removing kanamycin through adsorption
A kanamycin and corncob technology, which is applied in adsorption water/sewage treatment, water/sludge/sewage treatment, other chemical processes, etc., can solve the problems of low adsorption capacity, poor selectivity of antibiotics, lack of antibiotics, etc. The effect of strong selection, strong anti-interference ability and high adsorption capacity
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[0044] (1) 500 grams of corncobs are placed in a pulverizer to pulverize, and sieved with sieves with apertures of 4mm and 6mm respectively to obtain corncobs with a particle size of 4 to 6mm;
[0045] (2) 85 grams of corn cobs obtained by step (1) are washed with 500 mL of deionized water and then soaked in 500 mL of absolute ethanol for 1 hour. After filtering, the liquid is removed to obtain substance P. After substance P is washed with 350 mL of deionized water To obtain substance P1, put substance P1 into 500mL of NaOH solution with a molar concentration of 3.7mol / L and soak for 1 hour, remove the liquid after filtration to obtain substance P2, and obtain substance P3 after substance P2 is washed with 500mL deionized water. Substance Q was obtained after being placed in a drying oven at 40°C for 36 hours;
[0046] (3) Add 12.96 grams of 2-fluoro-4-methyl-5-bromopyridine and 3.84 grams of 2-hydroxy-5-iodopyridine to 800 ml of absolute ethanol, stir for 5 minutes at 1000r / m...
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