Shale aperture measurement device and method based on imbibition and ion diffusion property
A technology of ion diffusion and measuring device, which is applied in the direction of measuring device, suspension and porous material analysis, permeability/surface area analysis, etc. It can solve the problems of large difference in pore size, difficulty in accurate measurement, high test cost, etc., and achieve low environmental impact , reliable results, and low cost of testing
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Embodiment 1
[0049] Example 1: see figure 1 , a shale pore size measurement device based on imbibition and ion diffusion characteristics, characterized in that it includes: a high-precision analytical balance 1, a support 2, a flask 3, a fishing line 4, a magnetic stirrer 5, a lifting system 6, a conductivity Rate meter 7, constant temperature and humidity box 8;
[0050] The high-precision analytical balance 1 is placed above the support 2 for measuring the mass change of the shale sample before and after water absorption; the precision of the high-precision analytical balance 1 is 0.0001g;
[0051] The support 2 is placed in the constant temperature and humidity box 8 for carrying the high-precision analytical balance 1; the middle of the support 2 is provided with a small hole for hanging the high-precision analytical balance 1 The shale sample is vertically suspended inside the support 2;
[0052] The flask 3 is placed on the upper surface of the magnetic stirrer 5 for containing dis...
Embodiment 2
[0058] Example 2: see figure 2 , a shale pore size measurement method based on imbibition and ion diffusion characteristics, comprising the following steps:
[0059] A. Extract cylindrical shale samples and calculate the cross-sectional area A c , seal the cylindrical surface of the cylindrical shale sample with epoxy resin, place it in a drying box and dry it until the quality of the cylindrical shale sample no longer changes;
[0060] B. Place the high-precision analytical balance on the support, hang the dried cylindrical shale sample on the high-precision analytical balance with a fishing line, and record the reading M0 of the high-precision analytical balance;
[0061] C. Place the lifting system under the support, place the flask on the magnetic stirrer, and place the magnetic stirrer on the lifting system;
[0062] D. Add volume V distilled water into the flask, and measure the conductivity G0 in the water;
[0063] E. Turn on the magnetic stirrer to raise the lifti...
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