PAFC (polyamuminum ferric chloride) liquid product and preparation method thereof
A technology of polyaluminum ferric chloride and liquid products, which is applied in chemical instruments and methods, cobalt halides, inorganic chemistry, etc., can solve the problems of slow speed, sodium hydroxide concentration, aluminum hydroxide precipitation, low efficiency, etc., and achieve shortening. Time-consuming, energy saving, high salinity effect
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[0027] In the preparation method of the polyaluminum ferric chloride liquid product of the present invention, while stirring, the sodium hydroxide solution is added into the mixed solution of aluminum chloride and ferric chloride in the form of spraying, which can effectively avoid the occurrence of precipitation caused by excessive local pH, greatly improving The time required for preparing the polyaluminum ferric chloride liquid product is shortened, and at the same time, a higher concentration of reaction raw materials can be used to prepare a high-concentration polyaluminum ferric chloride liquid product, which can save a lot of energy for the subsequent drying process.
[0028] Preferably, the preparation method of described aluminum chloride and ferric chloride mixed solution comprises:
[0029] Aluminum chloride and ferric chloride are mixed and stirred to be dissolved in a solvent to obtain a mixed solution of aluminum chloride and ferric chloride;
[0030] Or aluminum...
Embodiment 1
[0052] A preparation method of polyaluminum ferric chloride liquid product, comprising the steps of:
[0053] Analytical pure aluminum chloride is mixed with the aluminum chloride aqueous solution that concentration is 2mol / L, and analytical pure ferric chloride hexahydrate is mixed with the ferric chloride aqueous solution that concentration is 2mol / L for subsequent use;
[0054] The sodium hydroxide aqueous solution that concentration is 4mol / L is mixed with analytically pure sodium hydroxide;
[0055] Take 100mL of the above-mentioned aluminum chloride aqueous solution and ferric chloride aqueous solution and add them to a 1500mL beaker, stir for 1 minute at a stirring rate of 600r / min with a high-speed disperser to make them fully mixed;
[0056] Then adjust the stirring rate of the high-speed disperser to 1000r / min, turn on the sprayer and continuously spray 100mL of sodium hydroxide aqueous solution, and continue stirring for 20 minutes to obtain the polyaluminum ferric ...
Embodiment 2
[0058] A preparation method of polyaluminum ferric chloride liquid product, comprising the steps of:
[0059] Analytical pure aluminum chloride is mixed with the aluminum chloride aqueous solution that concentration is 4mol / L, and analytical pure ferric chloride hexahydrate is mixed with the ferric chloride aqueous solution that concentration is 4mol / L for subsequent use;
[0060] The sodium hydroxide aqueous solution that concentration is 4mol / L is mixed with analytically pure sodium hydroxide;
[0061] Take 100mL of the above aluminum chloride aqueous solution and ferric chloride aqueous solution and add them to a 1500mL beaker, stir with a high-speed disperser at a stirring rate of 800r / min for 3 minutes to make them fully mixed;
[0062] Then adjust the stirring rate of the high-speed disperser to 1200r / min, turn on the sprayer and continuously spray 210mL of sodium hydroxide aqueous solution, and continue stirring for 30 minutes to obtain the polyaluminum ferric chloride ...
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