Identification method of nitrogen-containing compounds in Maotai
A nitrogen compound and identification method technology, applied in the field of analysis and detection, can solve the problems of inaccurate composition and content of nitrogen-containing compounds, and achieve the effects of meeting the needs of rapid detection, simple operation and wide applicability
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[0019] This method mainly adopts headspace solid-phase microextraction combined with gas chromatography-nitrogen-phosphorus detector-mass spectrometry to rapidly detect and qualitatively quantify nitrogen-containing compounds in Moutai liquor. The specific steps are as follows:
[0020] 1) Extraction of nitrogen-containing compounds in Moutai liquor: First prepare a Moutai liquor sample, first dilute it with deionized water to a solution system with an alcohol content of 10%, then take 5 mL of the liquor sample, add 1 g of sodium chloride, 20 μL of 2-methoxyl 3-methylpyrazine was placed in a 20 mL headspace vial, and the headspace vial was sealed with a silicone gasket. The SPME conditions were as follows: insert the extraction head into the headspace vial, make the extraction head 2 cm above the sample, and use a constant temperature water bath. At a temperature of 50 °C, extract for 45 minutes; after the extraction is completed, quickly insert the extraction head into the inj...
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