Preparation method of infrared electrothermal film
An electric heating film and infrared technology, applied in the direction of electric heating devices, ohmic resistance heating, electrical components, etc., can solve the problems of large attenuation, unstable power, small working temperature range, etc., and achieve small radiation heat loss and heat transfer thermal resistance Small, the effect of improving the utilization rate
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Embodiment 1
[0021] Take by weighing the graphene powder of 6 weight parts, the far-infrared emission agent of 0.5 weight part, the binding diluent of 3 weight parts, at first the graphene powder is mixed with the far-infrared emission agent and stirred evenly, then add the binding diluent and mix Finally, a slurry is formed; the bonding diluent is a high temperature resistant phenolic resin, and the particle size of the graphene powder is 30-60nm.
[0022] The slurry is evenly coated on the surface of the substrate to form a film, and the first electrothermal film is formed after drying or drying, wherein the thickness of the first electrothermal film is controlled at 5 μm.
[0023] SnCl 4 .5H 2 O, ethanol, HF, H 3 PO 4 Mix and stir with deionized water according to the mass ratio of 50:12:4:5:25 to obtain a stirred mixed liquid, wherein the stirring time is 3 hours.
[0024] The stirred mixture was refluxed for 1 h in a reflux tube at 70°C.
[0025] The refluxed mixed solution was a...
Embodiment 2
[0028] Take by weighing the graphene powder of 7 weight parts, the far-infrared emission agent of 2 weight parts, the binding diluent of 5 weight parts, at first the graphene powder is mixed with the far-infrared emission agent and stirred evenly, then add the binding diluent and mix Finally, a slurry is formed; the bonding diluent is a high temperature resistant phenolic resin, and the particle size of the graphene powder is 30-60nm.
[0029] The slurry is uniformly coated on the surface of the substrate to form a film, and the first electrothermal film is formed after drying or drying, wherein the thickness of the first electrothermal film is controlled at 15 μm.
[0030] SnCl 4 .5H 2 O, ethanol, HF, H 3 PO 4 Mix and stir with deionized water according to the mass ratio of 65:20:6:8:35 to obtain a stirred mixed liquid, wherein the stirring time is 5 hours.
[0031] The stirred mixture was refluxed in the reflux tube at 90°C for h.
[0032] The refluxed mixed solution wa...
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