A transition state iron-based heavy metal immobilization reagent and preparation method thereof
A transition state and heavy metal technology, applied in chemical instruments and methods, agriculture, organic fertilizers, etc., to achieve the effect of easy permanent removal and long-term stable fixation
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[0044] The preparation method of immobilization reagent is as follows:
[0045] 1. Disperse the attapulgite powder in deionized water and treat it with ultrasonic waves for 5 minutes, wherein the mass ratio of solid to liquid is 1:20 to obtain a dispersed powder suspension;
[0046] 2. Add the dispersed powder suspension to the hydrochloric acid solution for acid treatment, wherein the mass percentage concentration of the hydrochloric acid solution is 5%, the stirring temperature is 30°C, and the stirring time is 1h. The mass ratio of the dispersed powder suspension to the hydrochloric acid solution is 1:20;
[0047] 3. The powder after acid treatment was washed twice with deionized water and absolute ethanol respectively, filtered and dried, and the drying temperature was 30°C;
[0048] 4. Disperse the dried powder I in the soluble iron salt solution and keep stirring, wherein the solid-to-liquid mass ratio of powder I to the iron salt solution is 1:20, the pH of the solution ...
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