A kind of preparation method of joint sealing material
A technology of sealing materials and raw materials
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[0031] The technical solution of the present invention is a preparation method of a joint filling and sealing material, including the following steps:
[0032] A preparation
[0033] 1) Part A: (parts by weight)
[0034] Polyether polyol DL-2000D 60-80
[0035] Polyether polyol EP-330N 10-30
[0036] Diphenylmethane diisocyanate MDI-50 10-20
[0037] 2) Part B: (parts by weight)
[0038] Polyether polyol EP-330N 30-60
[0039] Chlorinated Paraffin-52 50-60
[0040] Amine chain extender (MOCA) 5
[0041] Organometallic catalyst 1
[0042] Talc 80
[0043] Softeners and defoamers 14
[0044] B. Preparation
[0045] Add the polyether polyol in the first component into the container, stir, heat up to 60-80°C, add MDI-50, heat up to 80°C, react at 80±2°C for 2h, and determine when the NCO content of the system reaches the predetermined value , Stop the reaction. After the reaction is completed, the temperature is lowered and vacuum degassing for 30 minutes, and the material is discharged to obtain ...
Embodiment 1
[0070] Follow the steps A, B, D, and E described in the above specific embodiment. among them:
[0071] A preparation
[0072] 1) Part A: (parts by weight)
[0073] Polyether polyol DL-2000D 60
[0074] Polyether polyol EP-330N 10
[0075] Diphenylmethane diisocyanate MDI-50 10
[0076] 2) Part B: (parts by weight)
[0077] Polyether polyol EP-330N 30
[0078] Chlorinated Paraffin-52 50
[0079] B. Preparation
[0080] Add the polyether polyol in component A into the container, stir, and heat to 60°C;
[0081] After the component B is stirred and dispersed evenly, it is heated to 100°C.
Embodiment 2
[0083] Repeat Example 1 but,
[0084] A preparation
[0085] 1) Part A: (parts by weight)
[0086] Polyether polyol DL-2000D 80
[0087] Polyether polyol EP-330N 30
[0088] Diphenylmethane diisocyanate MDI-50 20
[0089] 2) Part B: (parts by weight)
[0090] Polyether polyol EP-330N 60
[0091] Chlorinated Paraffin-52 60
[0092] B. Preparation
[0093] Add the polyether polyol in the first component into the container, stir, heat up to 80°C, add MDI-50, heat up to 80°C, after the reaction is completed, cool down and degas in vacuum for 20 minutes;
[0094] After the component B is stirred and dispersed evenly, it is heated to 110°C and dehydrated under vacuum for 2 hours.
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