Preparation method of X-type molecular sieve/LDHs composite adsorbent for separating methane and nitrogen through pressure swing adsorption
A methane separation and pressure swing adsorption technology, which is applied in the preparation of adsorbents and composite adsorbents, can solve the problems of less research and development of activated carbon adsorbents, difficulty in meeting the requirements for selective separation of methane/nitrogen adsorption, and achieve easy implementation, The effect of mild reaction conditions and enhanced adsorption effect
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Embodiment 1
[0018] A preparation method of an X-type molecular sieve / LDHs composite adsorbent for separating methane and nitrogen by pressure swing adsorption, comprising the following steps:
[0019] 1) Weigh 150gAl(NO 3 ) 3 9H 2 O and 51.3gMg(NO 3 ) 2 ·6H 2 O was dissolved in 1200 mL of deionized water to make a total concentration of 0.5 mol L -1 Mixed salt solution, weigh 80g NaOH and dissolve in 400ml deionized water to prepare 5mol L -1 Add the NaOH solution drop by drop to the mixed salt solution under stirring conditions, keep the pH value of the system at 9-10 during the dropwise addition, continue stirring and aging for 3 hours after the NaOH solution is added dropwise, and the obtained product Filter, wash with deionized water repeatedly 3 times, and place in a constant temperature drying oven at 100°C for 6 hours to obtain a hydrotalcite sol with a solid content of 2 wt%.
[0020] 2) Weigh 100g of NaX molecular sieve with a thickness of 0.1-1μm and add it to 500ml of po...
Embodiment 2
[0024] A preparation method of an X-type molecular sieve / LDHs composite adsorbent for separating methane and nitrogen by pressure swing adsorption, comprising the following steps:
[0025] 1) Weigh 150gAl(NO 3 ) 3 9H 2 O and 51.3gMg(NO 3 ) 2 ·6H 2 O was dissolved in 1200 mL of deionized water to make a total concentration of 0.5 mol L -1 Mixed salt solution, weigh 80g NaOH and dissolve in 400ml deionized water to prepare 5mol L -1 Add the NaOH solution drop by drop to the mixed salt solution under stirring conditions, keep the pH value of the system at 9-10 during the dropwise addition, continue stirring and aging for 3 hours after the NaOH solution is added dropwise, and the obtained product Filter, wash with deionized water repeatedly 3 times, and place in a constant temperature drying oven at 100°C for 6 hours to obtain a hydrotalcite sol with a solid content of 2 wt%.
[0026] 2) Weigh 100g of 0.1-1μm NaX molecular sieve and add it to 500ml of sodium dodecylbenzenes...
Embodiment 3
[0030] A preparation method of an X-type molecular sieve / LDHs composite adsorbent for separating methane and nitrogen by pressure swing adsorption, comprising the following steps:
[0031] 1) Weigh 150gAl(NO 3 ) 3 9H 2 O and 51.3gMg(NO 3 ) 2 ·6H 2 O was dissolved in 1200 mL of deionized water to make a total concentration of 0.5 mol L -1 Mixed salt solution, weigh 80g NaOH and dissolve in 400ml deionized water to prepare 5mol L -1 Add the NaOH solution drop by drop to the mixed salt solution under stirring conditions, keep the pH value of the system at 9-10 during the dropwise addition, continue stirring and aging for 3 hours after the NaOH solution is added dropwise, and the obtained product Filter, wash with deionized water repeatedly 3 times, and place in a constant temperature drying oven at 100°C for 6 hours to obtain a hydrotalcite sol with a solid content of 2 wt%.
[0032] 2) Weigh 50g of 0.1-1μm NaX molecular sieve and add it to 500ml of sodium lignosulfonate a...
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