Method for increasing sulfur content of sulfur-carbon composite through vulcanization accelerator
A technology of vulcanization accelerator and sulfur-carbon compound, which is applied in the field of electrochemical power supply, can solve the problem that it is difficult to efficiently increase the sulfur content of the sulfur-carbon compound, and achieves the effects of lowering temperature, simple equipment and increasing sulfur content
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Embodiment 1
[0036] (1) Mix polyacrylonitrile, elemental sulfur, and 2-mercaptobenzothiazole in a mass ratio of 1:1:0.1, and put them into a ball mill tank for ball milling at a speed of 400 rpm for 3 hours to obtain Mix the reaction mixture homogeneously;
[0037] (2) Put the reaction mixture into an airtight container, place it in a vacuum tube furnace, pass in argon gas, raise the temperature to 185°C, keep it warm for 1 hour, then continue to raise the temperature to 280°C, and keep it warm for 6 hours. The heating rate is 10°C / hour. After the reaction was completed, it was naturally cooled to room temperature.
Embodiment 2
[0045] (1) Mix polyacrylonitrile, elemental sulfur, and 2-mercaptobenzothiazole in a mass ratio of 1:3:0.1, and put them into a ball mill tank for ball milling at a speed of 400 rpm for 3 hours to obtain Mix the reaction mixture homogeneously;
[0046] (2) Put the reaction mixture into an airtight container, place it in a vacuum tube furnace, pass in argon gas, raise the temperature to 185°C, keep it warm for 1 hour, then continue to raise the temperature to 320°C, and keep it warm for 6 hours. The heating rate is 10°C / hour. After the reaction was completed, it was naturally cooled to room temperature.
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