Cool feeling hydrogel and preparation method thereof and cool feeling fabric and preparation method thereof
A cool-feeling fabric and hydrogel technology, applied in the field of textile fabrics, can solve the problems of affecting the state of motion, humidity and stuffiness, and poor cooling effect, and achieve the effect of increasing heat loss, lasting coolness, and lowering body temperature
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[0035] The embodiment of the present invention provides a method for preparing a cooling hydrogel, comprising the following steps:
[0036] A) under the effect of dispersant, peppermint oil and xylitol are mixed with water to obtain mixed solution;
[0037] B) mixing the mixed solution with N-vinylpyrrolidone, acrylamide, an initiator, a crosslinking agent and water, and performing in-situ free radical polymerization to obtain a cool-feeling hydrogel.
[0038] The invention adopts a coating process to prepare the cooling-feeling hydrogel, and the process flow mainly includes emulsification, polymerization, etc., and the method is simple and easy.
[0039] In the embodiment of the present invention, peppermint oil, xylitol, dispersant and water are mixed, preferably under the condition of stirring, to obtain a mixed solution by emulsification.
[0040]The present invention mainly uses peppermint oil and xylitol as ice-feeling raw materials, and the contents of the peppermint o...
Embodiment 1
[0063] (1) Add 5g pineapple mint oil (Turner AT), 10g lavender mint oil (Turner NM type), 5g xylitol (Turner NW product) and 10g dispersant GNS (Turner company) 300mL of deionized water, mixed at 90°C, and a mixed solution was obtained after 15 minutes; the mixed solution, 20g of N-vinylpyrrolidone and 10g of acrylamide were added to the In the 500mL four-necked flask, feed nitrogen at room temperature, stir for 15min, then add 0.5g / L initiator APS (Demei Company) and 1g / L crosslinking agent MBA (Demei Company) to the above-mentioned four-necked flask ) and water, stirred evenly, heated up to 70°C for in-situ radical polymerization, and kept for 3h. After the reaction, the obtained reactant was placed in an oven, dried at 70° C. to constant weight, and passed through a 200-mesh sieve to obtain a cool-feeling hydrogel with a particle size of 15 μm. Wherein, the total mass of the peppermint oil and xylitol is 20% of the cool feeling hydrogel mass.
[0064] According to the met...
Embodiment 2
[0071] (1) Add 7g pineapple mint oil (Turner AT), 12g lavender mint oil (Turner NM type), 8g xylitol (Turner NW product) and 10g dispersant GNS (Turner company) 300mL of deionized water, mixed at 70°C, and a mixed solution was obtained after 30 minutes; the mixed solution, 15g of N-vinylpyrrolidone and 8g of acrylamide were added to the In the 500mL four-necked flask, feed nitrogen at room temperature and stir for 18min, then add 0.8g / L initiator APS (Demei company) and 1.5g / L cross-linking agent MBA (Demei company) to the above-mentioned four-necked flask. company) and water, stirred evenly, heated up to 75°C for in-situ radical polymerization, and kept for 4h. After the reaction, the obtained reactant was placed in an oven, dried at 75° C. to constant weight, and passed through a 200-mesh sieve to obtain a cool-feeling hydrogel with a particle size of 10 μm. Wherein, the total mass of the peppermint oil and xylitol is 20% of the cool feeling hydrogel mass.
[0072] Accordi...
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