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Method for recycling acetylene from slag slurry

A technology of slurry and acetylene, which is applied in the parts of acetylene gas generators, acetylene generators, petroleum industry, etc., can solve problems such as environmental pollution, safety hazards, and enterprise losses, so as to reduce production costs, increase safety, Significant economic benefits

Inactive Publication Date: 2016-01-06
TIANJIN DAGU CHEM CO LTD
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  • Description
  • Claims
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Problems solved by technology

[0002] In the process of producing acetylene gas by the calcium carbide method, the acetylene generator in the original production process needs to continuously add water to the generator in order to prevent the reaction temperature from being too high, and in order to control the liquid level, it is necessary to pass the excess slurry water through the overflow pipeline The acetylene content in the discharged slurry is generally in the range of 300-400mg / kg. The slurry pipeline is an open pipeline, and a large amount of acetylene gas will be discharged into the atmosphere with the discharge of calcium carbide slurry, which not only pollutes the environment, but also brings pollution to the enterprise. cause losses, and there are certain security risks

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  • Method for recycling acetylene from slag slurry

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Embodiment Construction

[0008] attached by figure 1 It can be seen that in the present invention, the calcium carbide slurry overflowed from the generator of the acetylene station is recycled from the overflow to the slurry tank through a closed pipeline, and then pumped to the desorption tower through the slurry pump, and the negative pressure of the desorption tower is provided by a water ring vacuum pump. The vacuum degree is controlled at -80Kpa ~ -55Kpa, and the temperature of the slurry is controlled at 50°C ~ 60°C. Under this condition, the acetylene gas contained in the water can basically be completely recovered. The ring vacuum pump sends it to the steam-water separator, and the separated acetylene gas first enters the oxygen analyzer to measure its oxygen content, which is linked to the switch of the on-site automatic valve to control the direction of the subsequent acetylene gas. 1.8%, the program automatically opens the automatic valve of the acetylene gas tank; if the oxygen content is ...

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Abstract

A method for recycling acetylene from slag slurry comprises the steps that a vacuum desorption method is adopted to recycle acetylene gas, generator overflow is sent to a slag slurry tank through an airtight pipeline and then sent to a desorption tower through a slag slurry pump, and low pressure boiling desorption is conducted on carbide-slag slurry in the desorption tower; after the desorped acetylene gas is sent to a cooler to be cooled, the acetylene gas is sent to a steam-water separator through a water ring vacuum pump, a part of the acetylene gas enters an acetylene heat exchanger and enters an oxygen meter after being cooled, and if the measured oxygen content is higher than 1.8%, the acetylene gas opens an emptying valve and is emptied through a fire barrier; if the measured oxygen content is lower than 1.8%, the acetylene gas is sent to an acetylene header pipe to enter a gas cabinet through an acetylene buffer tank and a flow meter. Desorbed slag slurry enters a slag slurry buffer tank from the bottom of the desorption tower and is pumped to a thickener through a slag slurry buffer pump. According to the method for recycling the acetylene from the slag slurry, running of the technology is stable, and the benefit is obvious. Meanwhile, a generator overflow pipeline is airtight, and the problem that an original overflow well is openair and not safe is solved.

Description

technical field [0001] The invention relates to a device for recovering acetylene gas from calcium carbide slurry in the production process of calcium carbide polyvinyl chloride. Background technique [0002] In the process of producing acetylene gas by the calcium carbide method, the acetylene generator in the original production process needs to continuously add water to the generator in order to prevent the reaction temperature from being too high, and in order to control the liquid level, it is necessary to pass the excess slurry water through the overflow pipeline The acetylene content in the discharged slurry is generally in the range of 300-400mg / kg. The slurry pipeline is an open pipeline, and a large amount of acetylene gas will be discharged into the atmosphere with the discharge of calcium carbide slurry, which not only pollutes the environment, but also brings pollution to the enterprise. There are also certain security risks. Contents of the invention [0003...

Claims

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Application Information

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IPC IPC(8): C10H21/00
Inventor 陈东历庆祥姚建王佳宁
Owner TIANJIN DAGU CHEM CO LTD
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