A kind of strongly inhibited water-based drilling fluid and its preparation method and application
A water-based drilling fluid and drilling fluid technology, applied in the field of drilling fluid, can solve the problems of high pollution and high cost, and achieve the effect of enhancing filtration loss reduction ability and strong inhibition.
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Embodiment 1
[0032] First prepare N,N-dimethylallyl propane sulfonate.
[0033]Weigh 430g of N,N-dimethylallylamine (DA) into the reactor, then put it into a constant temperature water bath, heat and start stirring. Then weigh 122g of 1,3-propane sultone (PS), add it directly into DA, the reaction temperature is 45°C, stir and react for 3 hours to obtain N,N-dimethylallyl propane sulfonate (DAPS) crude products. Transfer the crude DAPS product to a large piece of filter paper, wrap it in a Soxhlet extractor, and use ethanol as a solvent to extract for 3 hours. After the extraction, put the filter paper bag in a drying box and dry it at 50°C to obtain Pure DAPS monomer with a yield of 94.3%.
Embodiment 2
[0039] Weigh 103gDAPS and 35gAM respectively, add a certain amount of deionized water to dissolve and transfer to the reactor, the total monomer concentration is 35%. Access to N 2 Deoxygenation was performed for 1 hour, and the temperature was raised to 60° C., kept for 30 minutes, and then 0.7 g of potassium persulfate was added. After 6 hours of reaction, a gel-like solid was obtained, which was precipitated with acetone to obtain a white precipitate. After drying at 110°C for 24 hours, it was pulverized to obtain a DAPS / AM zwitterionic copolymer.
Embodiment 3
[0041] Weigh 60gDAPS, 50gAM, 15gNaCl respectively, add a certain amount of deionized water to dissolve and transfer to the reactor, the total monomer concentration is 40%. Access to N 2 Deoxygenation was performed for 1 hour, and the temperature was raised to 55° C., kept for 30 minutes, and then 0.75 g of ammonium persulfate was added. After 5 hours of reaction, a gel-like solid was obtained, which was precipitated with acetone to obtain a white precipitate. After drying at 110°C for 24 hours, it was pulverized to obtain a DAPS / AM zwitterionic copolymer.
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