A kind of green bark extract for tobacco and its application
A technology of extract and green skin, applied in the fields of application, tobacco, food science, etc., can solve the problems of simple utilization of green skin, poor smoking experience of low-tar cigarettes, etc., and achieve important market development and application prospects, low cost, and equipment. simple effect
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Embodiment 1
[0029] Grind 500g of sun-dried green bark through a 20-mesh sieve, add 75% ethanol according to a solid-liquid ratio of 1:5 (g:mL), heat and reflux for extraction for 5 hours, filter to obtain the filtrate and filter residue, and distill the filtrate to remove the solvent under reduced pressure , to obtain the first concentrate; filter the obtained filter residue, add ethyl acetate according to a solid-liquid ratio of 1:3 (g:mL), heat and reflux for extraction for 1 h, filter, and distill off the solvent under reduced pressure to obtain the second concentrate; combine The obtained first concentrate and second concentrate are mixed concentrates; add deionized water to the mixed concentrate according to the ratio of solid to liquid of 1:1 (g:mL), heat to collect fractions, and collect them into the mixed concentrate When the weight reached 40%, stop collecting, and obtain the extract A15g of the bark bark of tobacco.
Embodiment 2
[0031] Grind 500g of sun-dried green bark through a 40-mesh sieve, add 75% ethanol according to a solid-liquid ratio of 1:10 (g:mL), heat and reflux for extraction for 10 hours, filter to obtain the filtrate and filter residue, and distill the filtrate to remove the solvent under reduced pressure , to obtain the first concentrate; filter the obtained filter residue, add ethyl acetate according to a solid-liquid ratio of 1:5 (g:mL), heat and reflux for extraction for 4h, filter, and distill off the solvent under reduced pressure to obtain the second concentrate; combine The obtained first concentrate and second concentrate are mixed concentrates; add deionized water to the mixed concentrate according to the solid-liquid ratio of 1:3 (g:mL), heat to collect fractions, and collect them into the mixed concentrate When the weight reaches 60%, the collection is stopped, and the extract B24g of the bark bark for tobacco is obtained.
Embodiment 3
[0033] Grind 500g of sun-dried green bark through a 60-mesh sieve, add 75% ethanol according to a solid-liquid ratio of 1:7.5 (g:mL), heat and reflux for extraction for 8 hours, and filter to obtain the filtrate and filter residue, wherein the filtrate is distilled off under reduced pressure to remove the solvent , to obtain the first concentrate; filter the obtained filter residue, add ethyl acetate according to the solid-liquid ratio of 1:4 (g:mL), heat and reflux for extraction for 2h, filter, and distill off the solvent under reduced pressure to obtain the second concentrate; combine The obtained first concentrate and second concentrate are mixed concentrates; add deionized water to the mixed concentrate according to the solid-liquid ratio of 1:2 (g:mL), heat to collect fractions, and collect them into the mixed concentrate Stop collecting at 50% of the weight, and get the green bark extract C19g for tobacco.
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