Method for extracting silymarin by using food-grade ethanol as an extracting solvent
A technology for extracting solvents and silymarin, which is applied in organic chemistry and other fields, and can solve problems such as blank preparation methods
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Embodiment 1
[0022] Example 1, Laboratory Extraction (Small Experiment).
[0023] (1) Use a screw oil press to extract most of the oil from the air-dried and air-dried milk thistle seeds, and put 500 grams of cake powder into a Soxhlet extractor.
[0024] (2) It is connected to the whole set of Soxhlet extractor and adopts the electric heating mantle heating system.
[0025] (3) Inject 1500-2000ml of food-grade ethanol from the top of the cooling tube of the Soxhlet extractor, and inject the ethanol through the cake powder (material layer) into the round bottom flask at the bottom (pumice is added in the flask to prevent bumping).
[0026] (4) Turn the control knob of the electric heating mantle, adjust the heating electric power, and increase the temperature slowly until the ethanol in the flask boils. At this time, ethanol vapor rises to the top cooler and begins to trickle into the material layer, and the time is started.
[0027] (5) Extract for 16 hours. After the last reflux is comp...
Embodiment
[0029] Embodiment 2, workshop-level production example.
[0030] (1) The oil extraction treatment of milk thistle seeds is as in Example 1.
[0031] (2) Take 1000kg of milk thistle cake powder and put it into a 1.3 cubic meter multifunctional extraction tank.
[0032] (3) Inject an appropriate amount of food-grade ethanol 1800kg from the liquid injection pipe on the top of the extraction tank, and the liquid level is higher than the upper edge of the material layer.
[0033] (4) Static immersion for 4 hours, open the liquid discharge valves on the top and bottom of the extraction tank, put the extract solution impregnated with cake powder into the evaporation tank at a certain flow rate, and at the same time, fresh solvent is drawn from the injection pipe on the top of the extraction tank to the tank The same flow rate of the bottom discharge liquid is injected into the material layer in the tank, so that the solvent entering and flowing out reaches a dynamic balance, and the...
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