A kind of reagent for detecting hair water and soy sauce and preparation method thereof
A technology for hair water and soy sauce, applied in biological testing, material inspection products, etc., can solve problems such as difficulty in distinguishing hair water and soy sauce, and achieve the effects of short detection time, obvious effect and simple use.
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[0037] Combine below figure 1 with 2 As shown, the synthesis process of the reagent for the detection of hair water and soy sauce in this embodiment is introduced in detail.
[0038] In this example, by first synthesizing 1,3,5,7-tetramethyl-8-phenyl-(2-nitro)-boron difluoride dipyrromethane (TMPB-o-N), and then synthesizing 1, 3,5,7-Tetramethyl-8-phenyl-(2-amino)-borondifluoride dipyrromethane (TMPB-o-A), and finally the test reagent of the present invention was obtained.
[0039] Specifically, first, accurately weigh 1.06 g (7.0 mmol) of o-nitrobenzaldehyde, dissolve it in 500 mL of dry CH 2 Cl 2 .
[0040] Next, under nitrogen protection, 1.44 mL (14.0 mmol) of 2,4-dimethylpyrrole was slowly added dropwise to the obtained solution while stirring. Afterwards, 1 drop of trifluoroacetic acid was added dropwise, the resulting solution was sealed, and kept stirring overnight at 25° C. until the substance spots of o-nitrobenzaldehyde had disappeared by detection by thin-laye...
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