Eluent for benzo[a]pyrene in soil and elution method thereof
An elution method and eluent technology are applied in the field of soil organic pollution treatment to achieve the effects of improving hard water resistance, improving solubilization effect and convenient operation.
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Embodiment 1
[0022] Example 1 The elution effect of low concentration benzo[a]pyrene contaminated soil
[0023] The composition of the soil eluent is: 3.0g / L Tween80, 1.0g / L SDS, 1.0g / L K 2 SiO 3 , the solvent is water.
[0024] Preparation of contaminated soil: Dissolve a certain amount of benzo[a]pyrene in dichloromethane solvent to fully dissolve it, and spray it evenly into the sterilized soil, place it at room temperature to volatilize the organic solvent in the soil, add sterile Water was used to make the soil moisture content reach 30%, and benzo[a]pyrene simulated contaminated soil with a concentration of 1.24mg / kg was prepared, which was placed in a sterile dark environment for aging for 1 month.
[0025] Elution method: Accurately weigh 8.0g of benzo[a]pyrene contaminated soil into a 200ml Erlenmeyer flask, add 80ml of prepared soil eluent and mix well (solid-liquid ratio 1:10), seal 1. After wrapping with aluminum foil, place the Erlenmeyer flask in an air bath constant tempe...
Embodiment 2
[0028] Example 2 The elution effect of high concentration benzo[a]pyrene contaminated soil
[0029] The composition of soil eluent is: Tween80 of 4.0g / L, SDS of 1.0g / L, K of 1.0g / L 2 SiO 3 , the solvent is water.
[0030]Preparation of contaminated soil: Dissolve a certain amount of benzo[a]pyrene in dichloromethane solvent to make it fully dissolved, evenly spray it into the sterilized soil, let it dry naturally to volatilize the organic solvent in the soil, add sterile water to make the soil The water content reaches 30%, and the benzo[a]pyrene simulated contaminated soil with a concentration of 68.24mg / kg is prepared, which is placed in a sterile dark environment for aging for 1 month.
[0031] Elution method: Accurately weigh 8.0g of benzo[a]pyrene contaminated soil into a 200ml Erlenmeyer flask, add 120ml of prepared soil eluent and mix well (solid-liquid ratio 1:15), seal 1. After wrapping with aluminum foil, place the Erlenmeyer flask in an air bath constant temperat...
Embodiment 3
[0034] Example 3 The elution effect of benzo[a]pyrene polluted aging soil
[0035] The composition of soil eluent is: Tween80 of 4.0g / L, SDS of 1.0g / L, K of 1.0g / L 2 CO 3 , the solvent is water.
[0036] Preparation of contaminated soil: Dissolve a certain amount of benzo[a]pyrene in dichloromethane solvent to fully dissolve it, and spray it evenly into the sterilized soil, place it at room temperature to volatilize the organic solvent in the soil, add sterile Water was used to make the soil moisture content reach 30%, and benzo[a]pyrene simulated contaminated soil with a concentration of 68.24mg / kg was prepared, which was placed in a sterile dark environment for aging for 6 months.
[0037] Elution method: Accurately weigh 8.0g of benzo[a]pyrene contaminated soil into a 200ml Erlenmeyer flask, add 120ml of prepared soil eluent and mix well (solid-liquid ratio 1:15), seal 1. After wrapping with aluminum foil, place the Erlenmeyer flask in an air bath constant temperature sh...
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