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Nano coating fiber active fracturing fluid

A technology of nano-coating and nano-composite fibers, which is applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve problems such as failure to achieve fracturing effects, limit construction scale, and affect fracturing effects, so as to improve portability. Sand performance, reduction of filtration loss rate, and easy configuration process

Inactive Publication Date: 2015-04-08
CHONGQING INST OF GEOLOGY & MINERAL RESOURCES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The commonly used active water fracturing fluid is generally composed of water, anti-swelling agent (commonly used potassium chloride) and drainage aid (usually a compound of surfactants, commonly used drainage aids in oil fields include D-60 and HP-8, etc.) Prepared according to a certain ratio, the active water fracturing fluid exhibits the following defects during fracturing construction: (1) high frictional resistance, which limits the construction displacement, thereby limiting the construction scale and affecting the fracturing effect; (2) The sand-carrying performance is poor, and the fractures are often not supported well, and the expected fracturing effect cannot be achieved.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Embodiment 1 Preparation of fracturing fluid of the present invention

[0039] Add 10% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and heat up to 80°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 2 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200-mesh sieve to obtain organic montmorillonite.

[0040] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 200°C at a ratio of 1:9 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 5%. pellets.

[0041] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump speed to 14r / mi...

Embodiment 2

[0043] Embodiment 2 Preparation of fracturing fluid of the present invention

[0044] Add 11% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and raise the temperature to 70°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 3 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200mesh sieve to obtain organic montmorillonite.

[0045] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 210°C at a ratio of 1:9 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 6%. pellets.

[0046] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump sp...

Embodiment 3

[0048] Embodiment 3 Preparation of fracturing fluid of the present invention

[0049] Add 12% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and heat up to 90°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 4 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200mesh sieve to obtain organic montmorillonite.

[0050] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 180°C at a ratio of 1:11 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 7%. pellets.

[0051] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump speed to 14r / mi...

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Abstract

The invention belongs to the technical field of shale gas well fracturing increase production, and particularly relates to a nano coating fiber active fracturing fluid. The invention aims at providing a fracturing fluid system having an integrated function of swelling prevention, resistance reduction and high sand carrying capacity, which is favorable for the fracturing modification construction of shale gas reservoir. According to the technical scheme, the nano coating fiber active water fracturing fluid is formed by compounding an antiswelling agent, a resistance reducing agent, nano coating fibers and water. The invention also provides a compounding method of the nano coating fiber active water fracturing fluid. The fracturing fluid has an antiswelling and resistance reduction effect, the sand carrying performance of the fracturing fluid is improved, the deposition way is changed, and the deposition rate of a supporting agent is reduced; and the filter loss is effectively reduced, and the damage rate for the shale reservoir is low. The compounding process is simple and easy, the damage for the shale reservoir is small, and the nano coating fiber active fracturing fluid is easy to flow back.

Description

technical field [0001] The invention belongs to the technical field of shale gas well fracturing and production stimulation, and in particular relates to a nano-coated fiber active water fracturing fluid with excellent anti-swelling, drag-reducing and sand-carrying performances for shale gas well fracturing construction. Background technique [0002] According to the hydraulic fracturing experience of shale gas wells in North America and China, active water is the most used liquid during fracturing construction, and other liquids including clean fracturing fluid and fiber fracturing fluid are also used in certain applications. The main purpose of choosing the active water liquid system instead of the commonly used cross-linked fracturing fluid is to reduce the damage of the shale reservoir, increase the complexity of the fracturing fracture network and the stimulated volume, and increase the production of shale gas wells as much as possible. The active water fracturing fluid...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68
CPCC09K8/68C09K8/885C09K2208/08C09K2208/12C09K2208/28
Inventor 张烨程礼军张劲陆朝晖张健强潘林华张义
Owner CHONGQING INST OF GEOLOGY & MINERAL RESOURCES
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