Nano coating fiber active fracturing fluid
A technology of nano-coating and nano-composite fibers, which is applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve problems such as failure to achieve fracturing effects, limit construction scale, and affect fracturing effects, so as to improve portability. Sand performance, reduction of filtration loss rate, and easy configuration process
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Embodiment 1
[0038] Embodiment 1 Preparation of fracturing fluid of the present invention
[0039] Add 10% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and heat up to 80°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 2 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200-mesh sieve to obtain organic montmorillonite.
[0040] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 200°C at a ratio of 1:9 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 5%. pellets.
[0041] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump speed to 14r / mi...
Embodiment 2
[0043] Embodiment 2 Preparation of fracturing fluid of the present invention
[0044] Add 11% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and raise the temperature to 70°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 3 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200mesh sieve to obtain organic montmorillonite.
[0045] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 210°C at a ratio of 1:9 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 6%. pellets.
[0046] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump sp...
Embodiment 3
[0048] Embodiment 3 Preparation of fracturing fluid of the present invention
[0049] Add 12% (mass fraction, the same below) montmorillonite aqueous solution into the reaction kettle, stir and heat up to 90°C, add an appropriate amount of hexadecyltrimethylammonium chloride aqueous solution dropwise, stir vigorously for 12 hours, and then add 2% silane The coupling agent was reacted for 4 hours, and the product was dried in an oven at a certain temperature to a constant weight, and pulverized by a pulverizer through a 200mesh sieve to obtain organic montmorillonite.
[0050] Organic montmorillonite (MMT) and polypropylene (PP) were extruded at a twin-screw at 180°C at a ratio of 1:11 to obtain a PP / MMT composite material, and then PP was added twice to blend to obtain a sample with a MMT content of 7%. pellets.
[0051] Put the obtained nanocomposite pellets into the melt spinning machine, adjust the temperature in Zone 1 to Zone 7 to 160°C to 210°C, the pump speed to 14r / mi...
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