Purifying device of amino acid

A technology of amino acid and purification section, which is applied in the field of purification equipment for extracting amino acids, which can solve problems such as easy bonding, high energy consumption, and high labor intensity, and achieve the effect of increasing the total yield and quality

Active Publication Date: 2015-04-01
JIANGSU YUANYANG PHARMA
View PDF12 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In many production processes, inorganic salts may usually be contained in amino acid mother liquor, and conventional processes are often purified by concentration or solvent, due to (NH4) 2 SO 3 , (NH4) 2 SO 4 、Na 2 SO 3 with Na 2 SO 4 It is very easy to bond, and the separation of amino acids and inorganic salts is difficult to achieve the desired effect. The whole process directly affects the yield, so the production cost is high, the energy consumption is large, and the labor intensity is high.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Purifying device of amino acid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] First open the water collection valve 45, then place the amino acid mother liquor containing 10% amino acid in the amino acid mother liquor collection bucket 11, wherein the amino acid is γ-aminobutyric acid, the inorganic salt is sodium sulfate, and the amino acid mother liquor is kept at a temperature of 20°C 1. Utilize the primary high-pressure pump 12 to send in the primary chromatographic column 13 through the delivery pipe, and the pressure of the primary high-pressure pump 12 is 0.01 MPa; observe the data on the primary liquid chromatograph 14 and show that the amino acid begins to flow out, starting from the primary high-pressure pump 12 Then start timing, open the amino acid collection valve 41 in the collection section after 10.5min, the high-concentration amino acid liquid flows from the discharge pipe to the amino acid collection bucket 42, continue to observe the numerical display of the primary liquid chromatograph 14, and the amino acid concentration decrea...

Embodiment 2

[0044] First open the water collection valve 45, and then place the amino acid mother liquor containing 15% amino acid in the amino acid mother liquor collection barrel 11, wherein the amino acid is aminoacetic acid, the inorganic salt is ammonium sulfate, and the amino acid mother liquor is at a temperature of 50° C. The high-pressure pump 12 is sent to the primary chromatographic column 13 through the liquid delivery pipe, and the pressure of the primary high-pressure pump 12 is 0.01 MPa; observing the data on the primary liquid chromatograph 14 shows that amino acids begin to flow out, and the timing starts after the primary high-pressure pump 12 is turned on After 10.5min, the amino acid collection valve 41 in the collection section is opened, and the high-concentration amino acid solution flows from the discharge pipe to the amino acid collection barrel 42. Continue to observe the numerical display of the primary liquid chromatograph 14, and the amino acid concentration is ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a purifying device of an amino acid. The purifying device comprises a primary purifying section, a pre-purifying section, a post-purifying section and a collecting section, wherein an amino acid mother liquid is firstly subjected to separation and purification through the primary purifying section, and is subjected to online monitoring through a primary liquid chromatograph; high-concentration amino acid liquid of which the amino acid mass fraction is higher than 99.0% is directly introduced into the collecting section to collect; the residual primary amino acid liquid is introduced into the pre-purifying section to be purified again; the effluent primary inorganic salt is introduced into the post-purifying section to be purified again, the mixed amino acid is separated out, and finally the separated liquid is collected. According to the purifying device, the amino acid mother liquid can be separated and purified; the concentration of the amino acid in the purified amino acid liquid is higher than 99.0%; and the amino acid is thoroughly separated from the inorganic salt.

Description

technical field [0001] The invention relates to the technical field of organic chemical synthesis and separation, in particular to a purification device for extracting amino acids from amino acid mother liquor. Background technique [0002] Amino acid is a general term for a class of organic compounds containing amino and carboxyl groups. Amino acid is the basic unit of protein, which endows protein with a specific molecular structure and makes its molecules biochemically active. Protein is an important active molecule in organisms, including enzymes that embrittle metabolism. In nature, there are more than 300 kinds of amino acids. [0003] ?Amino acids are mainly used in medicine to prepare compound amino acid infusions, and are also used as therapeutic drugs and synthetic peptide drugs. At present, there are more than 100 kinds of amino acids used as medicines, including 20 kinds of amino acids that make up proteins and more than 100 kinds of amino acids that make up no...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): B01D15/10
Inventor 王建峰任举陈文如
Owner JIANGSU YUANYANG PHARMA
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products