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A high-temperature, high-pressure corrosion resistance reaction experimental device and a method for using the reaction kettle system thereon

An experimental device, high temperature and high pressure technology, applied in the direction of measuring devices, sampling devices, instruments, etc., can solve the problems of difficult control of temperature and pressure, inability to sample online, insufficient sealing, etc., achieve good heat preservation effect, strong corrosion resistance, and easy disassembly Effect

Inactive Publication Date: 2016-03-30
CHINA UNIV OF PETROLEUM (EAST CHINA)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The purpose of the present invention is to provide a high-temperature and high-pressure corrosion-resistant reaction experimental device, which solves the problems of the existing high-temperature and high-pressure reaction kettles, such as bulky kettle body, laborious disassembly, insufficient sealing, difficult temperature and pressure control, and inability to take samples online.

Method used

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  • A high-temperature, high-pressure corrosion resistance reaction experimental device and a method for using the reaction kettle system thereon
  • A high-temperature, high-pressure corrosion resistance reaction experimental device and a method for using the reaction kettle system thereon
  • A high-temperature, high-pressure corrosion resistance reaction experimental device and a method for using the reaction kettle system thereon

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Embodiment

[0024] Example: such as Figure 1 ~ Figure 3 As shown, the present invention includes gas supply system, piston container 3A, reactor system 4A and control system 5A;

[0025] The gas supply system includes a high-pressure gas cylinder 1A and a gas booster pump 2A, through which the injected reaction liquid is used to simulate the formation water used for organic acid generation or the organic acid used for simulated dissolution is transported from the piston container 3A to the reactor system 4A, and the pump The flow range is 0.01-10mL / min, the maximum output pressure is 50MPa, and the pump head is made of Hastelloy material, so it can withstand certain acid and alkali liquids. The piston container 3A is installed on the base 1', and the piston container 3A includes a piston 6' and a cylinder body 7'. Plugs 8' are installed at both ends of the cylinder body 7', and sealing rings 3' are installed on the plugs 8'. The end is provided with a pressure cap 9'; the cylinder cavit...

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Abstract

The invention discloses an experimental device for high temperature and high pressure anti-corrosion reaction, and belongs to the technical field of high temperature and high pressure anti-corrosion reaction. An existing high temperature and high pressure reaction kettle has the defects that a kettle body is heavy, is difficult to detach and is insufficiently sealed, the temperature and the pressure are unlikely to control, and the on-line sampling cannot be realized. The experimental device for the high temperature and high pressure anti-corrosion reaction comprises an air supply system, a piston container, a reaction kettle system and a control system. Various materials can generate chemical reaction in the experiment device in a high temperature and high pressure range of 50MPa pressure and 350 DEG C temperature; components, such as a piston, a cylinder body, an end cap, the reaction kettle body and a sampler, directly in contact with a reaction solution are made from a hastelloy material so as to have the strong corrosion resistance. The experimental device has functions of temperature and pressure presetting, and temperature and pressure overload protection; meanwhile, the experimental device is provided with electromagnetic propelled stirring blades which can be used for stirring reactors during reaction, so that the reaction speed is increased; furthermore, the experimental device is provided with the sampler so as to realize the on-line sampling on the reaction solution.

Description

technical field [0001] The invention belongs to the technical field of high-temperature and high-pressure corrosion-resistant reactions, and in particular relates to a high-temperature and high-pressure corrosion-resistant reaction experimental device for simulating the generation and dissolution reaction of organic acids under geological conditions. Background technique [0002] The successful exploration and development of tight oil in North America has led to an upsurge in unconventional oil and gas exploration. Tight oil has become a new field of global unconventional oil and gas exploration and development, and the secondary pores formed by the dissolution of organic acids on tight oil reservoirs are the main storage space for tight oil. Existing studies on the dissolution of tight reservoirs are mainly focused on tight sandstones but are not related to the formation of organic acids. Therefore, the research on the formation and dissolution of organic acids is of great ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N33/00G01N1/10G01N1/22
Inventor 李吉君曲希玉王伟明阴建新张亚念
Owner CHINA UNIV OF PETROLEUM (EAST CHINA)
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