Concrete with high water reducing rate, water reducing agent used and preparation method thereof
A concrete water-reducing agent and water-type technology, which is applied in the field of concrete with high water-reducing rate, can solve the problems of sensitive dosage, poor mud tolerance, etc., and achieves easy operation, small loss over time, and good adaptability Effect
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[0027] According to the composition of Table 1, the hydrophobic polymer concrete water reducer is prepared, and the steps include:
[0028]
[0029]
[0030] (1) Add polyhydric alcohol containing 3-8 carbon atoms to acrylic acid monomer, then add catalyst sodium dodecylbenzenesulfonate, heat to dissolve, and then perform esterification reaction at 90-105°C for 4-7h , make acrylate; Wherein, the molar ratio of polyhydric alcohol and acrylic acid monomer is 1:2-4;
[0031] (2) Add deionized water to the product of step (1), heat it to fully dissolve, and make a reaction bottom solution; then add hydrophobic surfactant and chain transfer agent, and stir at 50-60°C Add hydrogen peroxide dropwise for copolymerization reaction, the reaction time is 2-3 hours, then keep warm at 25-30°C and continue to stir for 1 hour; finally use sodium hydroxide aqueous solution to adjust the pH value to 7-8 to obtain a solid content of 35-40%. Hydrophobic polymer concrete superplasticizer. ...
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