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Method for detecting source of oxide scale peeled off from inner wall of heated surface of boiler

An inspection method and oxide skin technology, which is applied in the direction of material analysis by measuring secondary emissions, can solve the problems of waste and time-consuming of steel pipes

Inactive Publication Date: 2015-03-04
XIAN THERMAL POWER RES INST CO LTD
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  • Claims
  • Application Information

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Problems solved by technology

[0004] The object of the present invention is to provide a method for inspecting the origin of scale peeling off on the inner wall of the heating surface of the boiler. The detection method is simple and convenient, and overcomes the defects that the traditional method is time-consuming, laborious, and causes a great waste of steel pipes that can still be used.

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  • Method for detecting source of oxide scale peeled off from inner wall of heated surface of boiler
  • Method for detecting source of oxide scale peeled off from inner wall of heated surface of boiler
  • Method for detecting source of oxide scale peeled off from inner wall of heated surface of boiler

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Embodiment Construction

[0024] The present invention will be described in further detail below in conjunction with the accompanying drawings and embodiments.

[0025] The first step is to randomly select scales that are bright gray on one side and black or dark gray on the other side from the scale peeled off on the inner wall of the tube panel on the heating surface of the boiler; when selecting scales, all scales that are obviously different in shape or color should be Inclusive, the number of picks should be no less than 3 pieces each.

[0026] In the second step, observe the black or dark gray side of the oxide scale with a scanning electron microscope equipped with an X-ray energy spectrometer to find the flaky inner layer residues of the oxide scale, and perform X-ray energy spectroscopy on the oxide scale inner layer residues. Spectrum analysis; flaky oxide skin inner layer residue, the composition of the oxide skin inner layer residue has trace elements in addition to Fe and O;

[0027] The ...

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Abstract

The invention relates to a method for detecting a source of a piece of oxide scale peeled off from the inner wall of a heated surface of a boiler. The method comprises the steps of selecting a piece of oxide scale with a light grey surface and a black or dark grey surface, observing the black or dark grey surface of the oxide scale by utilizing a scanning electronic microscope with an X-ray energy dispersive spectrometer, finding out residues on an inner layer of the oxide scale, and carrying out X-ray energy spectral analysis on the residues on the inner layer of the oxide scale so as to obtain an X-ray energy spectral analysis result; and comparing the X-ray energy spectral analysis result of the residues on the inner layer of the oxide scale with an alloy steel element in a tubular screen of the heated surface, and determining the source of the peeled oxide scale. By adopting the method, the oxide scale peeled off from the tubular screen can be easily and conveniently determined to be peeled from the inner wall of which material, so that the peel-off and pipe blockage problem of the oxide scale can be treated in a targeted manner in a power plant.

Description

technical field [0001] The invention belongs to the field of material detection and analysis, and in particular relates to a method for inspecting the source of scale peeled off on the inner wall of a heating surface of a boiler. Background technique [0002] The thermal power generation unit operates in a long-term high-temperature environment. The boiler superheater and reheater tubes are oxidized by high-temperature water vapor to form scales. Due to the large difference between the linear expansion coefficients of the scales and the matrix, it is easy Peeling is blocked at the lower elbow. At present, the peeling and blocking of pipes on the high-temperature heating surface of coal-fired generator sets has become the most important reason for unplanned shutdown of the unit. [0003] The medium temperature of the boiler superheater and reheater gradually increases from the inlet to the outlet. In order to reduce the cost, the manufacturer generally combines a variety of a...

Claims

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Application Information

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IPC IPC(8): G01N23/22
Inventor 唐丽英周荣灿贾建民郭岩张周博李季李江
Owner XIAN THERMAL POWER RES INST CO LTD
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