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Method for measuring axial heat conductivity of one-dimensional material

A measurement method and thermal conductivity technology, applied in the field of nanomaterials, can solve the problems of expensive equipment and complex optical signal process, and achieve the effect of reversible effect.

Active Publication Date: 2015-02-18
INST OF PHYSICS - CHINESE ACAD OF SCI
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Problems solved by technology

[0006] In terms of optical performance measurement, due to the extremely small size of one-dimensional materials, the interaction area with light is very small, so the absorption cross-section and scattering cross-section are very small. According to the existing experimental equipment, the process of accurately detecting the optical signal of one-dimensional materials is complicated and difficult. The equipment required is expensive

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  • Method for measuring axial heat conductivity of one-dimensional material
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  • Method for measuring axial heat conductivity of one-dimensional material

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Embodiment Construction

[0039] The "one-dimensional material" referred to in the present invention is a nano-scale one-dimensional material or a micron-scale one-dimensional material, wherein the nano-scale one-dimensional material includes nanowires, nanotubes, nanobelts, nanofibers or nanorods.

[0040] In order to solve the need for precise positioning accuracy when measuring the thermal conductivity of extremely small-sized one-dimensional materials, it is difficult to achieve small-sized detection accuracy and spatial accuracy with traditional infrared thermometers, and the macroscopic scale The contact of a temperature probe with a one-dimensional material is likely to cause a huge change in the temperature of the material itself. The invention provides a method for measuring the thermal conductivity of a one-dimensional material. The measuring method includes: forming a wrapped section and a bare section adjacent to the wrapped section on the one-dimensional material. Wherein, at the wrapping ...

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Abstract

The invention discloses a method for measuring axial heat conductivity of a one-dimensional material. The method comprises the following steps: forming a coating section and an exposed section adjacent to the coating section on the one-dimensional material, wherein the one-dimensional material is coated with a coating material different from the one-dimensional material on the coating section, and the one-dimensional material is exposed to an ambient environment on the exposed section; heating the one-dimensional material until the one-dimensional material reaches a thermal stabilization balance state; obtaining the positions at first and second reference points on the one-dimensional material and the temperatures in the thermal stabilization balance state at the first and second reference points, wherein the first reference point is an adjacent point at the adjacent part of the coating section and the exposed section, and the second reference point is another reference point, which is different from the adjacent point, of the exposed section; and calculating to obtain the heat conductivity according to the positions and the temperatures at the first and second reference points and based on a calculation relationship between pre-established heat conductivity and the positions and the temperatures at the first and second reference points. The disappearance edges of volatile substances are utilized as temperature indication coordinates, the measurement accuracy is high, and the measurement difficulty is reduced.

Description

technical field [0001] The invention relates to the technical field of nanometer materials, in particular to a method for measuring axial thermal conductivity of one-dimensional materials. Background technique [0002] One-dimensional materials, especially one-dimensional nanomaterials, are materials that are extremely small in two geometric dimensions and approach or reach the macroscopic level in the other geometric dimension. This material has special excellent mesoscopic properties that some macroscopic materials do not have, such as excellent electrical properties that are highly sensitive to structure, and thermal and optical properties that are superior to macroscopic materials. Therefore, this material has broad application prospects. [0003] However, due to its extremely small size, its morphology can only be characterized by expensive equipment such as scanning electron microscopes or even transmission electron microscopes, and the steps are cumbersome, which req...

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Application Information

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IPC IPC(8): G01N25/20G01N25/18G06F19/00B82Y35/00
Inventor 张霄周维亚解思深
Owner INST OF PHYSICS - CHINESE ACAD OF SCI
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