Crease resisting agent for cotton and preparation method and application of crease resisting agent for cotton
A technology of anti-wrinkle agent and condensation reaction, which is applied in the field of anti-wrinkle agent for cotton and its preparation, which can solve the problems that the anti-wrinkle performance of the finished fabric is not involved, and achieve the effects of remarkable anti-wrinkle effect, enhanced firmness, improved wrinkle resistance and washability
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Embodiment 1
[0032] 1. Dissolution of cyanuric chloride
[0033] In a reaction flask equipped with a stirrer and a thermometer, add cyanuric chloride [select 20.24g (0.1mol)], and dissolve it with a mixture of acetone and ice water [select 20mL ice water and 10mL acetone] (i.e., acetone aqueous solution) , and mechanically stirred for 10 minutes to promote its full dissolution.
[0034] 2. Add m-phenylenediamine disulphonic acid [choose 13.4g (0.05mol)] into 40mL water, under the condition of stirring, slowly (3min) add sodium carbonate (0.05mol) powder equal to the substance amount, after the sodium carbonate powder is added , and continue to stir for 5 minutes, so that the m-phenylenediamine disulphonic acid becomes sodium m-phenylenediamine disulphonate, and a sodium m-phenylenediamine disulphonate solution is obtained.
[0035] 3. Slowly add m-phenylenediamine disulphonate sodium solution dropwise into the three-necked flask dissolved with cyanuric chloride system to carry out the fir...
Embodiment 2
[0046] 1. Dissolution of cyanuric chloride
[0047] In a reaction flask equipped with a stirrer and a thermometer, add cyanuric chloride [select 20.24g (0.1mol)], and dissolve it with a mixture of acetone and ice water [select 20mL ice water and 10mL acetone] (i.e., acetone aqueous solution) , and mechanically stirred for 10 minutes to promote its full dissolution.
[0048] 2. m-Phenylenediamine disulphonic acid [choose 13.4g (0.05mol)] into 40mL of water, under the condition of stirring, slowly add sodium carbonate (0.05mol) powder of the same amount, after adding the sodium carbonate powder, continue stirring For 5 minutes, the m-phenylenediamine disulphonic acid was converted into sodium m-phenylenediamine disulphonate to obtain a sodium m-phenylenediamine disulphonate solution.
[0049] 3. Slowly add m-phenylenediamine disulphonate sodium solution dropwise into the three-necked flask dissolved with cyanuric chloride system for the first condensation, the reaction temperat...
Embodiment 3
[0054] 1. Dissolution of cyanuric chloride
[0055] In a reaction flask equipped with a stirrer and a thermometer, add cyanuric chloride [select 20.24g (0.1mol)], and dissolve it with a mixture of acetone and ice water [select 20mL ice water and 10mL acetone] (i.e., acetone aqueous solution) , and mechanically stirred for 10 minutes to promote its full dissolution.
[0056] 2. m-Phenylenediamine disulphonic acid [choose 13.4g (0.05mol)] into 40mL of water, under the condition of stirring, slowly add sodium carbonate (0.05mol) powder of the same amount, after adding the sodium carbonate powder, continue stirring For 5 minutes, the m-phenylenediamine disulphonic acid was converted into sodium m-phenylenediamine disulphonate to obtain a sodium m-phenylenediamine disulphonate solution.
[0057] 3. Slowly add m-phenylenediamine disulphonate sodium solution dropwise into the three-necked flask dissolved with cyanuric chloride system for the first condensation, the reaction temperat...
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