Synthesis and separation method of trans-seven-membered-cucurbituril
A seven-membered melon ring, separation method technology, applied in the direction of organic chemistry, etc., to achieve the effect of simple and fast method
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[0019] Embodiment: The synthetic implementation method of trans seven-membered melon ring iQ[7]:
[0020] Weigh 50 grams of glycoside urea, 20 grams of paraformaldehyde, 200 mL of concentrated hydrochloric acid, reflux for 6 hours, cool, and dilute with water step by step until no precipitation occurs (the precipitation is eight-membered melon ring Q[8], six Yuan melon ring Q[6] and other poorly soluble melon rings, about 40 grams). Concentrate the mother liquor containing five-membered melon ring Q[5], seven-membered melon ring Q[7], a small amount of spliced fourteen-membered melon ring tQ[14], and trans seven-membered melon ring iQ[7] to a certain volume ( It should not be too viscous, so as not to affect the sample on the column, take 25 mL of the concentrated solution (0.9-1.1 grams of solid per mL). Load the concentrated solution on a chromatography column with silica gel G as the stationary phase (diameter: 40mm; height: 800mm) , with 1:1:0.01~0.3 water: acetic acid:...
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