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Preparation method of phase change fibers

A phase-change fiber and fiber technology, which is applied in fiber treatment, chemical instruments and methods, heat exchange materials, etc., can solve problems such as difficulties, low melting viscosity of phase-change substances, and complicated operation, so as to improve the temperature adjustment effect and effectively The effect of high content and simple process

Active Publication Date: 2014-04-09
CHINA LEATHER & FOOTWEAR IND RES INST
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Problems solved by technology

The hollow fiber impregnation method is to impregnate the hollow fiber in the phase change material solution, fill the hollow part with the phase change material, and then seal the ends of the fiber. The disadvantage is that the hollow fiber impregnation method has difficulty in sealing the end, and requires a larger inner diameter of the hollow fiber. The phase change material remains on the surface of the fiber, so it is easy to ooze and wash out; in the melt composite spinning method, the melt viscosity of the low temperature phase change material is low, and there is no spinnability. It is difficult to simply use the phase change material for melt composite spinning. After adding plasticizer, it can be used for spinning, but the conditions are harsh and the operation is complicated; the coating method is a simple and easy method to fix the phase change substance on the fabric, but it will affect the air permeability of the textile; the microcapsule composite spinning method is Add a certain amount of phase change material microcapsules to the spinning solution, and extrude through the spinneret to make fibers. This method is expensive and the effective content of the phase change material is low; the polymer graft modification method also has complex operations. , the disadvantage of low effective content of phase change materials

Method used

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  • Preparation method of phase change fibers

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Embodiment Construction

[0019] see Figure 5 , a specific process flow of the present invention is, put the hollow fiber 4 of 6.67dtex * 64mm into the liquid storage tank 2, add the paraffin phase-change material 5 that melting point is 32 ℃ in the liquid storage tank 2, and press the pressing plate 3; Put the liquid storage tank 2 into the vacuum chamber 1, then seal the vacuum chamber 1, and evacuate the vacuum chamber 1; stop vacuuming when the vacuum degree reaches -0.09MPa, and raise the temperature of the vacuum chamber to 65°C; After the change material 5 is completely melted, ensure that the hollow fiber 4 is completely immersed below the liquid level of the phase change material 5, open the valve of the vacuum chamber 1, and let air enter the vacuum chamber 1, and the phase change material 5 enters the hollow fiber 4 under the action of the external atmospheric pressure The interior of the hollow fiber 4 is fixed under the capillary action of the inner hole of the hollow fiber 4; the hollow ...

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Abstract

The invention provides a preparation method of phase change fibers. The preparation method comprises the following steps: putting hollow fibers in a liquid storage tank, adding phase change materials to the liquid storage tank, and pressing by using a pressing plate; putting the liquid storage tank in a vacuum bin, sealing the vacuum bin, and vacuumizing the vacuum bin; heating the vacuum bin so as to ensure that the temperature in the vacuum bin is higher than the melting point of the phase change materials so as to melt the phase change materials; stopping vacuumizing, and opening a valve of the vacuum bin so as to ensure that the phase change materials enter inner parts of the hollow fibers under the effect of external atmospheric pressure and are fixed under the capillarity action of inner holes of the hollow fibers; and taking out the hollow fibers filled with the phase change materials, and removing the phase change materials adhered to the surfaces of the hollow fibers, thus obtaining the phase change fibers with a temperature control effect. The preparation method has the advantages that the phase change materials are directly poured into the inner parts of the hollow fibers and are fixed through the capillarity action of the hollow fibers, compared with a microcapsule method, the preparation method is simple in process and low in cost, the effective content of the phase change materials is high, and the temperature adjusting effect can be substantially improved.

Description

technical field [0001] The invention relates to a preparation method of a phase-change fiber, in particular to a phase-change fiber used for shoemaking and clothing cloth, and belongs to the field of phase-change heat storage materials. Background technique [0002] Phase change fiber is a new type of functional product that combines phase change material technology with fiber manufacturing technology, and has two-way temperature regulation. When the temperature of the external environment rises, the phase change material contained in the fiber undergoes a phase change, from solid to liquid, absorbing heat and storing it inside the fiber; when the temperature of the external environment decreases, the phase change material changes from liquid to solid, releasing heat. The stored heat keeps the body surface temperature and keeps the human body in a comfortable state. [0003] The temperature adjustment mechanism of phase change fiber textiles is different from that of tradit...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/02C09K5/06
Inventor 石飞
Owner CHINA LEATHER & FOOTWEAR IND RES INST
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