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Extraction method of roselle red color

An extraction method, roselle red technology, applied in the field of natural pigment extraction technology, can solve the problems of increased sewage treatment costs, prolonged concentration time, organic solvent residue, etc., achieve good value for further processing, reduce pectin content, The effect of reducing viscosity

Active Publication Date: 2014-03-26
婺源县聚芳永茶业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The problems in the above method are: due to the use of organic solvents to extract roselle red pigment, there will inevitably be problems such as environmental pollution, organic solvent residues, high cost, and high energy consumption.
In other extraction methods of roselle red pigment, a large amount of pectin substances are inevitably extracted, which makes the viscosity of the extract solution at a relatively high level and affects subsequent production. Chitosan is used to absorb and centrifuge before processing through plate and frame microfiltration. The process is too long, and the loss of the pigment process is large; the direct filtration of pectin by ultrafiltration is very easy to cause blockage of ultrafiltration membrane pores, the cleaning frequency of membrane elements will increase, and the cleaning agent may remain in the filtrate, cleaning agent and eluate It will also increase the cost of sewage treatment
During the concentration process, the high temperature of vacuum concentration will lead to the instability of roselle red pigment; the resin adsorption requires the use of organic solvents during elution, which is costly and also has the problem of organic solvent residues; single-stage reverse osmosis membrane concentration, when mass production The medium concentration time will be prolonged, and its optimal dehydration temperature will cause rapid growth of microorganisms, especially in a long period of time, microbial factors will lead to a reduction in pigment content

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] A process for extracting rosellin, the steps of which are as follows:

[0038] 1) Material selection: select 1500 kg of roselle raw materials, remove calyxes that are damaged by diseases and insect pests, and moldy calyxes;

[0039] 2) Drying: using a microwave dryer as the heat source, the roselle calyx was dried using a two-step drying method; the first drying temperature was 130 °C for 5 min; the second drying temperature was 60 °C , the time is 120 min, the dry roselle calyx weight after treatment is 525kg, and its water content is 10%;

[0040] 3) Pulverization: crush the dried roselle calyx to 20 meshes with a pulverizer;

[0041]4) Extraction: Pour the crushed roselle raw materials into a continuous extraction tank group consisting of 3 extraction tanks, 175kg / tank, and the purified water with a pH of 6.5 enters the subsequent extraction tanks sequentially from one extraction tank, hot water The temperature was 65°C, the extraction time was 120 min, and 2100 kg...

Embodiment 2

[0049] A process for extracting rosellin, the steps of which are as follows:

[0050] 1) Material selection: Select 1000kg of roselle raw materials, remove calyxes that are damaged by diseases and insect pests, and moldy calyxes.

[0051] 2) Drying: The heat source is a hot air dryer, and the roselle calyx is dried according to the two-step drying method; the drying temperature of the first step is 90°C for 30 minutes; the drying temperature of the second step is 40°C, The time is 300min, and the roselle dry calyx weight after processing is 354kg, and its water content is 12%;

[0052] 3) Pulverization: crush the dried roselle calyx to 4 meshes with a pulverizer;

[0053] 4) Extraction: Pour the crushed roselle raw material into a continuous extraction tank group consisting of two extraction tanks, 177kg / tank, and purified water with a pH of 4.0 enters the subsequent extraction tank from one extraction tank, and the temperature of the hot water is 50 ℃, leaching time 300min,...

Embodiment 3

[0060] A process for extracting rosellin, the steps of which are as follows:

[0061] 1) Material selection: select 3000 kg of roselle raw materials, remove calyxes that are damaged by diseases and insect pests, and moldy calyxes;

[0062] 2) Drying: use a dryer with a microwave as the heat source, and use a two-step drying method to dry the roselle calyx; the first drying temperature is 150°C for 3 minutes; the second drying temperature is 80°C , the time is 30 min, the dry roselle calyx weight after treatment is 1038kg, and its water content is 11%;

[0063] 3) Pulverization: pulverize the dried roselle calyx with a pulverizer to 4-40 mesh;

[0064] 4) Extraction: Pour the crushed roselle raw materials into a continuous extraction tank group consisting of 6 extraction tanks, 173kg / can, and the purified water with a pH of 6.8 enters the subsequent extraction tanks in sequence from the first extraction tank. The hot water temperature is 65 °C, the extraction time is 120 min,...

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PUM

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Abstract

The invention discloses an extraction method of roselle red color. The method comprises the steps of selecting materials, drying, smashing, digesting, enzyme treatment, clarifying, concentrating, blending, sterilizing and drying. Compared with the prior art, the method has the advantages that low pigment loss rate is ensured in a raw material drying process, the unit raw material utilization efficiency and pigment extraction rate are increased, the problem of thickness of an extracting solution is solved in a mild way, the stability of pigments in a processing process is ensured, the processing cost is reduced remarkably, and the product quality is enhanced. The method contributes to saving energy and protecting the environment, is friendly to the ecological environment, does not cause any adverse effect, and is a novel processing process which is worthy of popularization for natural plant pigments.

Description

[0001] technical field [0002] The invention relates to a process for extracting natural pigments, in particular to a method for extracting roselle red pigments. [0003] Background technique [0004] Roselle, also known as roselle, mountain eggplant, etc., is an annual shrub of the Malvaceae Hibiscus genus. It was first produced in Africa and is a plant in tropical and subtropical arid areas. It is planted in Fujian, Guangxi, Guangdong, Yunnan and other places in my country. Roselle has a plump appearance, thick petals, purple-red and black calyx, bright and fresh melted water, slightly fragrant air, and sour taste, which contains a large amount of organic acids, vitamin C, protein, various amino acids, natural vitamins, and iron, which are needed by the human body. Minerals such as calcium and phosphorus. [0005] As people's awareness of health care gradually increases, consumers are more and more concerned and worried about the food safety of synthetic food coloring, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B61/00
Inventor 杨晓东周军陈悦水
Owner 婺源县聚芳永茶业有限公司
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