Conducting carbon fiber composite material as well as preparation method thereof
A technology of conductive carbon fiber and composite material, applied in the field of conductive carbon fiber composite material and its preparation
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Embodiment 1
[0016] 1) Graphene is dispersed in ethanol, and preparation concentration is the graphene ethanol solution of 0.01g / L, then, then, use the ultrasonic equipment that power is 1000W to carry out ultrasonic processing 0.5 hour to described graphene ethanol solution, obtain graphene ethanol solution;
[0017] 2) Add copper nanowires and epoxy resin to the graphene ethanol solution obtained in step 1) so that the concentration is 20g / L and 200g / L respectively to obtain a mixed solution, and stir the mixed solution with a magnetic stirrer for 30 minutes, then Then use an ultrasonic device with a power of 1000W to carry out ultrasonic treatment on the mixed solution for 0.5 hours;
[0018] 3) Put the ultrasonically treated mixed solution in step 2) into an oven with a temperature of 80 degrees Celsius, bake for 10 hours, and then use a vacuum pump to extract the ethanol solvent in the mixed solution until the mixed solution has no bubbles;
[0019] 4) Add a chemically equivalent cur...
Embodiment 2
[0022] 1) Graphene is dispersed in ethanol, and preparation concentration is the graphene ethanol solution of 1g / L, then, then, use the ultrasonic equipment that power is 300W to carry out ultrasonic treatment to described graphene ethanol solution for 5 hours, obtain graphene ethanol solution ;
[0023] 2) Add copper nanowires and epoxy resin to the graphene ethanol solution obtained in step 1) so that the concentration is 59g / L and 200g / L respectively to obtain a mixed solution, and stir the mixed solution for 5 minutes with a magnetic stirrer, then Then use an ultrasonic device with a power of 300W to carry out ultrasonic treatment on the mixed solution for 0.5 hours;
[0024] 3) Put the ultrasonically treated mixed solution in step 2) into an oven with a temperature of 50 degrees Celsius, bake for 48 hours, and then use a vacuum pump to extract the ethanol solvent in the mixed solution until the mixed solution has no bubbles;
[0025] 4) Add a chemically equivalent curing...
Embodiment 3
[0028] 1) Graphene is dispersed in ethanol, and preparation concentration is the Graphene ethanol solution of 0.2g / L, then, then, use the ultrasonic equipment that power is 600W to carry out ultrasonic treatment 2 hours to described Graphene ethanol solution, obtain Graphene ethanol solution;
[0029] 2) Add copper nanowires and epoxy resin to the graphene ethanol solution obtained in step 1) to make the concentrations 40.0g / L and 200g / L respectively to obtain a mixed solution, and stir the mixed solution with a magnetic stirrer for 20 minutes, Then use an ultrasonic device with a power of 800W to carry out ultrasonic treatment to the mixed solution for 3 hours;
[0030] 3) Put the ultrasonically treated mixed solution in step 2) into an oven with a temperature of 80 degrees Celsius, bake for 30 hours, and then use a vacuum pump to extract the ethanol solvent in the mixed solution until the mixed solution has no bubbles;
[0031] 4) Add a chemically equivalent curing agent to...
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