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Smooth processing device and smooth processing method of CL-20 grains

A CL-20, processing device technology, used in explosives processing equipment, offensive equipment, explosives, etc., can solve the problems of high cost, high cost, and difficulty in applying high-sensitivity energetic materials, and achieve reliable and smooth processing, safe and smooth. processing effect

Active Publication Date: 2013-10-23
BEIJING INSTITUTE OF TECHNOLOGYGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] There are also reports of using ultrasonic waves to smooth graphite particles, but this method has the disadvantages of high energy consumption and low output
More importantly, this method is difficult to apply to high-sensitivity energetic materials. Due to the penetration of high-intensity ultrasonic energy, it is easy to expand the tiny defects inside the crystal particles, forming cavities / holes inside the crystal particles, giving Energetic material particles pose potential hazards in practical use
[0006] Supercritical fluid technology is a better technology that can be applied to the processing of energetic materials. However, this method has the characteristics of small output and high cost (high production cost and equipment cost), which is not conducive to industrialization and practical application
[0007] For now, recrystallization (including solvent erosion method) is usually used to smooth explosive particles, but recrystallization needs to consume a lot of organic solvents or strong acids, which not only increases the cost, but also is harmful to the health of workers and the environment Protect
More importantly, the explosive particles obtained by the recrystallization method are only particles with a relatively regular crystal form. From a microscopic point of view, there are still edges and corners of the crystal particles at the edges and other positions, and the obtained particles are not real smooth particles.

Method used

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  • Smooth processing device and smooth processing method of CL-20 grains
  • Smooth processing device and smooth processing method of CL-20 grains
  • Smooth processing device and smooth processing method of CL-20 grains

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Experimental program
Comparison scheme
Effect test

specific Embodiment approach

[0079] The specific implementation method of CL-20 particle smooth processing of the present invention is as follows:

[0080] raw material:

[0081] PTFE grinding ball: Density: 2.1g / cm 3 ; Shore D hardness: 55HD; Manufacturer: Nanjing Ives Chemical Products Co., Ltd.

[0082] Fluorosilicone rubber grinding ball: Density: 1.4g / cm 3 ; Shore A hardness: 70HA; Manufacturer: Chengdu Senfa Rubber & Plastic Co., Ltd.

[0083] Acetone: commercially available

Embodiment 1

[0085] 1. Weigh 2kg of polytetrafluoroethylene smooth grinding balls and add them to the grinding chamber of the smooth grinding equipment. The diameter of the grinding balls is 4mm, and the filling rate of the grinding chamber grinding balls is 75%; weigh 1.2kg of aged grinding balls of fluorosilicone rubber Add it into the aging chamber of the stirring aging equipment, the diameter of the aging grinding ball is 3mm, and the filling rate is 55%.

[0086] 2. Prepare the distilled aqueous solution of acetone as the grinding solvent liquid, and the weight percent concentration of acetone is 4%.

[0087] 3. Weigh 4kg of raw material CL-20, measure 9.3Kg of grinding solvent solution, fully mix the raw material CL-20 and grinding solvent to form a uniformly mixed slurry, and the concentration of CL-20 slurry is 30%wt.

[0088] 4. Input the uniformly mixed CL-20 slurry into the grinding chamber of the smooth processing equipment and the aging chamber of the stirring aging equipment ...

Embodiment 2

[0092] 1. Weigh 1.75kg polytetrafluoroethylene smooth grinding balls and add them to the grinding chamber of the smooth grinding equipment. The diameter of the grinding balls is 4mm, and the filling rate of the grinding chamber is 65%; Into the aging cavity of the stirring aging equipment, the aging grinding ball diameter is 3mm, and the filling rate is 50%.

[0093] 2. Prepare the distilled aqueous solution of acetone as the grinding solvent liquid, and the weight percent concentration of acetone is 4%.

[0094] 3. Weigh 4kg of raw material CL-20, measure 9.3Kg of grinding solvent solution, fully mix the raw material CL-20 and grinding solvent to form a uniformly mixed slurry, and the concentration of CL-20 slurry is 30%wt.

[0095] 4. Input the uniformly mixed CL-20 slurry into the grinding chamber of the smooth processing equipment and the aging chamber of the stirring aging equipment for circular smoothing treatment. The speed of the agitator in the smooth grinding chamber...

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Abstract

The invention provides a smooth processing device and a smooth processing method of CL-20 grains. The device comprises smooth grinding equipment, and agitating and ageing equipment, wherein a discharging opening of a smooth grinding cavity is connected with a feeding opening of an agitating and ageing cavity through a pipeline; a discharging opening of the agitating and ageing cavity is connected with a feeding opening of the smooth grinding cavity through a pipeline; the position of the pipeline, which is close to the agitating and ageing cavity, is provided with a discharging valve; a material circulating pump is arranged on the pipeline behind the position. Slurry formed by uniformly mixing the raw materials CL-20 and a grinding solution and slurry is conveyed into the smooth processing device to be circularly processed between the smooth grinding cavity and the agitating and ageing cavity; the CL-20 slurry which is sufficiently grinded and aged is discharged and then is filtered in vacuum and dried to finally obtain a CL-20 product with smooth grains. According to the smooth processing device and the smooth processing method disclosed by the invention, methods of wet-method agitating and grinding and solvent dissolving are effectively combined; the device and the method are simple to operate and high in safety; the production efficiency is high; the smooth processing of the CL-20 grains with high mechanical sensitivity can be realized.

Description

technical field [0001] The invention relates to a technology for smoothing energetic material particles, and more specifically, to a device and method for smoothing CL-20 particles. Background technique [0002] With the development of science and technology and the increasingly fierce confrontation of weapons, the smooth processing technology of energetic materials is in the ascendant at home and abroad. Because the smooth treatment of the morphology or structure of energetic material particles can not only effectively improve the fluidity and packing density of energetic materials, but also effectively reduce their mechanical sensitivity and shock wave sensitivity. Therefore, the smooth fine explosive particles will play an important role in practical applications. [0003] CL-20 (hexanitroazaisowurtzitane) is an organic high-energy compound with a density 8% higher than Octogen (HMX), a detonation velocity 6% higher, and an energy density higher than 15%. It will be used...

Claims

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Application Information

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IPC IPC(8): C06B21/00
Inventor 郭学永张朴焦清介张静元杨毅
Owner BEIJING INSTITUTE OF TECHNOLOGYGY
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