A kind of heavy oil hydrogenation catalyst containing bauxite ore and its preparation and application
A heavy oil hydrogenation and catalyst technology, applied in the direction of organic compound/hydride/coordination complex catalyst, physical/chemical process catalyst, petroleum industry, etc. Catalytic effect, good effect of heavy oil hydrogenation catalytic activity
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Embodiment 1
[0028] Weigh 38g of diesel oil, add 1.0g of organic bentonite (Jiangsu Huate New Material Co., Ltd., the mass fraction of organic matter is 20-35%), and homogenize with a shearing machine. Add 1.0 g of analytically pure oleic acid, then heat and stir on an 80° C. oil bath for 1 h. The obtained homogeneous mixed oil was cooled to room temperature, 0.5 g of PEG 600, 0.2 g of sodium dodecylbenzenesulfonate, and 0.5 g of analytically pure ethylene glycol were added to homogenize at room temperature to obtain dispersion medium A.
Embodiment 2
[0030] Weigh 42 g of kerosene, add 1.0 g of organic bentonite (Jiangsu Huate New Material Co., Ltd., the mass fraction of organic matter is 20-35%), and homogenize with a shearing machine. Add 1.2g of analytically pure oleic acid, heat to 70°C and stir for 2h. After cooling to room temperature, 0.2 g of sodium oleate, 0.4 g of PEG2000, and 1.0 g of analytically pure ethanol were added. Stir evenly at high speed to obtain dispersion medium B.
Embodiment 3
[0032] Take bauxite powder whose average particle size is less than 20 μm, weigh 3.0 g and place it in a test tube. Weigh 5.0g of dispersion medium A into the same test tube, stir and vibrate with a glass rod, wait for the powder to infiltrate evenly, and let it stand for 24 hours without obvious sedimentation. Catalyst C1 is obtained.
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