High-uniformity quantitative splitting and subpackaging technology of standard coal sample

A standard sample and homogeneity technology, which is used in the preparation of coal standard samples and the quantitative reduction and sub-packaging process of coal standard samples with high uniformity. High uniformity effect

Inactive Publication Date: 2013-08-07
PEOPLES REPUBLIC OF CHINA QINHUANGDAO ENTRY EXITINSPECTION & QUARANTINE BUREAU COAL INSPECTION TECHN CENT
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  • Summary
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Especially when the amount of divided coal is large, in order to reduce human error, mechanical methods should be used as much as possible. However, there is no unified standard for the shrinkage and packaging process of coal standard samples.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0016] The sample preparation and sub-packaging are carried out in a sample preparation room that meets the requirements of the coal sample preparation method (GB 474-2008), and the ambient temperature does not exceed 30°C and the relative humidity does not exceed 75%.

[0017] One-time shrinking and packaging:

[0018] Crush the selected coal sample after 600 kg of aging to prepare a suitable one-time sub-packing particle size <13 mm coal sample. The coal sample is piled and coneed, and the sample is scattered from the top of the sample pile in small portions to form a regular particle size distribution from the top to the bottom, from the center to the outer edge, and the pile is poured at least 3 times. Then gradually flatten or flatten it from top to bottom into a flat body with a thickness of about 40cm, and divide the coal sample into 8 equal sectors. Take coal samples of equal quality from each of the 8 sectors, mix them and add them to the rotating container-type mechanica...

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Abstract

The invention discloses a high-uniformity quantitative splitting and subpackaging technology of a standard coal sample, relating to the technical field of coal detection. The technology comprises the steps that a primary subpackaging fineness coal sample is stacked, doped, leveled and equally divided into N parts; coal samples with the equal mass are taken out from the N parts of coal samples, blended and split into N parts, and stored separately till all the coal samples are split into N parts; the N parts of coal samples are stacked, doped, leveled and equally divided separately; coal samples with the equal mass are taken out from the N parts of coal samples respectively, blended, split into N parts, and subpackaged till all the coal samples are split and subpackaged; the coal sample subjected to the primary splitting and subpackaging is broken into coal with the fineness for detection, then air-dried, divided into N parts, and spread in discs to form uniform rectangular blocks; each rectangular block is equally divided into small blocks with the mass greater than the minimum packaging unit mass of the coal samples; the coal samples with the minimum packaging unit mass are taken out from the identical small block coal samples in the N parts of coal sample discs respectively; and the N parts of coal samples are blended, split into N parts, and subpackaged into the minimum packaging units. The technology has the advantages that a great number of samples can be quantitatively split and packaged for one time, and the split and packaged samples have high uniformity.

Description

Technical field [0001] The invention relates to the technical field of coal detection, in particular to a high-uniformity quantitative shrinkage and packing process for coal standard samples, which is suitable for the preparation of coal standard samples. Background technique [0002] In coal inspection, usually only the repeatability and reproducibility are specified for the measurement results, that is, the precision is clearly specified. However, in order to provide reliable coal quality testing results, not only the precision but also the accuracy must be tested. Coal standard samples are one of the most commonly used methods for checking accuracy. Especially under the conditions of market economy, coal reference materials will play their special "measuring tool" role. Regular use of coal standard samples to calibrate instruments and use of coal standard samples to evaluate inspection data can find out whether the results of a certain characteristic index measured by the lab...

Claims

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Application Information

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IPC IPC(8): G01N1/28
Inventor 张衡米飞
Owner PEOPLES REPUBLIC OF CHINA QINHUANGDAO ENTRY EXITINSPECTION & QUARANTINE BUREAU COAL INSPECTION TECHN CENT
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