Method for preparing palm kernel shell activated carbon by catalytic activation
A catalytic activation and palm shell technology, applied in the field of activated carbon, can solve the shortage of raw materials and other problems, and achieve the effect of reusing, cost saving and huge economic benefits
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Embodiment 1
[0025] Example 1: Put 100g of raw material palm shell into a crucible and carry out anaerobic carbonization in a muffle furnace at 450°C for 1h, then take 10g of carbonized material and 5ml of potassium carbonate solution with a mass percentage concentration of 2% for immersion, and then carbonize The mass ratio of material and potassium carbonate impregnation is 100:1. After drying, it is placed in a tube furnace for activation for 1 hour at 850 ° C and a water vapor velocity of 1 g / min. Finally, it is washed and dried to obtain the product. Its methylene blue The adsorption value is 240 mg / g, and the iodine adsorption value is 1164 mg / g.
Embodiment 2
[0026] Embodiment 2: put 100g raw material into the crucible and carry out anaerobic carbonization in muffle furnace at 450 ℃ for 90min, then get 10g carbonized material and 5ml mass percent concentration and be 1.4% potassium carbonate solution impregnation, now carbonized material and The mass ratio of potassium carbonate in the impregnation solution is 100:0.7. After drying, place it in a tube furnace for activation for 1.5 hours at 850°C and a water vapor velocity of 1.5g / min, and finally wash and dry to obtain the product , its methylene blue adsorption value is 278mg / g, iodine adsorption value is 1268mg / g.
Embodiment 3
[0027] Embodiment 3: put 100g raw material into the crucible and carry out anaerobic carbonization in muffle furnace at 550 ℃ for 30min, then get 10g carbonized material and 5ml mass percent concentration and be 5% potassium carbonate solution impregnation, now carbonized material and The mass ratio of potassium carbonate in the impregnating solution is 100:2.5. After drying, place it in a tube furnace for activation for 0.5h at 950°C and a water vapor velocity of 2g / min, and finally wash and dry to obtain the product. Its methylene blue adsorption value is 245 mg / g, and iodine adsorption value is 1180 mg / g.
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