Tea polyphenol-containing chitosan-minced fillet protein composite film and preparation method thereof
A technology of chitosan and tea polyphenols, applied in the field of chitosan-surimi protein composite film and its preparation, to achieve good mechanical properties
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Embodiment 1
[0022] Weigh 1g chitosan and 1g frozen bighead carp surimi and dissolve in 50ml pH2.0 acetic acid solution, add 0.5g glycerin and 0.05g tea polyphenols (product purity 85%, purchased from Hangzhou Qinyuan Natural Plant Technology Co., Ltd.) Finally, stir at a constant speed for 10 minutes to obtain the chitosan-surimi protein film-forming solution; the film-forming solution was incubated at 70°C for 20min, and was centrifuged at a low speed at 3000rpm for 20min to remove air bubbles; the processed chitosan-surimi protein was formed into The film solution was evenly poured into a plexiglass plate frame of 100×100×10 mm, the film forming temperature was 60°C, and the film forming time was 6 hours. The prepared chitosan-surimi protein composite film containing tea polyphenols has a thickness of 0.128mm, a tensile strength of 12MPa, an elongation at break of 64%, a light transmittance of 78% at 600nm, and a water vapor transmission rate of 1.05× 10 -10 g / m×s×Pa, DPPH free radical...
Embodiment 2
[0024] Weigh 0.5g chitosan and 3g frozen silver carp surimi and dissolve in 50ml pH2.5 lactic acid solution, add 1g glycerin and 0.1g tea polyphenols (product purity 70%, purchased from Hangzhou Qinyuan Natural Plant Technology Co., Ltd.) Finally, stir at a constant speed for 10 minutes to obtain the chitosan-surimi protein film-forming solution; the film-forming solution was incubated at 50°C for 30min, and was centrifuged at a low speed at 3000rpm for 20min to remove air bubbles; the processed chitosan-surimi protein was formed into The film solution was evenly poured into a plexiglass plate frame of 100×100×10 mm, the film forming temperature was 40°C, and the film forming time was 12 hours. The prepared chitosan-surimi protein composite film containing tea polyphenols has a thickness of 0.124mm, a tensile strength of 25MPa, an elongation at break of 80%, a light transmittance of 74% at 600nm, and a water vapor transmission rate of 1.18×10 -10 g / m×s×Pa, DPPH free radical el...
Embodiment 3
[0026] Weigh 0.3g chitosan and 4g frozen hairtail surimi and dissolve in 50ml pH3.0 hydrochloric acid solution, add 0.5g glycerin and 0.05g tea polyphenols (product purity 80%, purchased from Hangzhou Qinyuan Natural Plant Technology Co., Ltd.) Finally, stir at a constant speed for 10 minutes to obtain the chitosan-surimi protein film-forming solution; the film-forming solution was incubated at 40°C for 50min, and was centrifuged at a low speed at 3000rpm for 20min to remove air bubbles; the processed chitosan-surimi protein was formed into The film solution was evenly poured into a plexiglass plate frame of 100×100×10 mm, the film forming temperature was 50°C, and the film forming time was 8 hours. The prepared chitosan-surimi protein composite film containing tea polyphenols has a thickness of 0.138mm, a tensile strength of 31MPa, an elongation at break of 89%, a light transmittance of 78% at 600nm, and a water vapor transmission rate of 1.17× 10 -10 g / m×s×Pa, DPPH free rad...
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