Warming agent clathrate compound applied to absorbent products and preparation method for warming agent clathrate compound
A technology of absorbent products and warming agents, applied in the field of packaging and objects, can solve the problems of high irritation and achieve long-lasting and optimized warmth
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Embodiment 1
[0063] To prepare clathrates, weigh 10g of β-cyclodextrin and place it in a reaction kettle, add 200ml of water and heat and stir until β-cyclodextrin is completely dissolved, and continue to heat up to 55°C to make a saturated aqueous solution; weigh 5g of ginger essential oil Dissolve with 5ml of propylene glycol, slowly add it into the reaction kettle with β-cyclodextrin under stirring condition, continue heating and stirring for 2h, concentrate the solution under reduced pressure to 50ml, refrigerate overnight at 4°C, filter out the precipitate, and place it at 90 After drying at ℃ for 1 hour, the cyclodextrin inclusion complex of ginger essential oil can be obtained, and the product is a white powder;
Embodiment 2
[0065] To prepare clathrates, weigh 15g of 2-hydroxypropyl-β-cyclodextrin and place it in a reaction kettle, add 200ml of water and heat and stir until 2-hydroxypropyl-β-cyclodextrin is completely dissolved, and continue to heat up to 70°C. Make a saturated aqueous solution; weigh 5g of vanillyl butyl ether and dissolve it in 5ml of ethanol, slowly add it into the reaction kettle containing 2-hydroxypropyl-β-cyclodextrin under stirring conditions, continue heating and stirring for 7h, while hot The precipitate was filtered out, and then dried at 90° C. for 1 hour to obtain the inclusion compound of vanillyl butyl ether cyclodextrin, which was a white powder.
Embodiment 3
[0067] To prepare clathrates, weigh 10g of β-cyclodextrin and place it in a reaction kettle, add 200ml of water and heat and stir until the β-cyclodextrin is completely dissolved, and continue to heat up to 75°C to make a saturated aqueous solution; weigh 2g of vanillin Dissolve -1,2-hexanediol acetal in 5ml PEG400, slowly add it into the reaction kettle containing β-cyclodextrin under stirring condition, continue heating and stirring for 1h, concentrate the solution under reduced pressure to 50ml, and refrigerate at 4°C Overnight, filter out the precipitate, and dry at 90°C for 1 hour to obtain the cyclodextrin inclusion compound of ginger essential oil, which is a white powder.
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