Sex attractant and trapping core for Dendrolimus tabulaeformis and preparation method of trapping core
A technology for pine caterpillars and attractants, which is applied in the directions of attracting pests, botanical equipment and methods, biocides, etc., can solve the problem that the sex pheromone lure core of pine caterpillars cannot be used universally, and can prevent and control the harm of pine caterpillars. , The effect of reducing labor costs and prolonging the validity period
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[0060] The preparation method of the above-mentioned pine caterpillar attractant lure core of the present invention includes: dissolving the pine caterpillar attractant in a solvent according to the above-mentioned composition and ratio, and then dripping it onto the septum of the sleeve-type composite rubber stopper with a syringe or Inside a polyethylene plastic tube.
[0061] Specific steps include:
[0062] (1) Prepare the sex attractant of Pinus tabulaeformis according to the following composition and ratio:
[0063] 1) cis 5, trans 7-dodecadiene acetate, 35-40%;
[0064] 2) cis 5, trans 7-dodecadienol, 35-40%;
[0065] 3) cis 5, trans 7-dodecadieacrylate, 2-18%;
[0066] 4) cis-5-dodecene acetate, 14-1%;
[0067] 5) cis-5-dodecenol, 14-1%;
[0068] Above percentage is that this compound accounts for the weight percent of attractant, mixes evenly according to above-mentioned proportion, for subsequent use;
[0069] (2) Dissolving the above-mentioned pine caterpillar...
Embodiment 1
[0083] The sex pheromone attractant lure core made in this embodiment adopts commercially available cis 5, trans 7-dodecadienol, cis 5, trans 7-dodecadienyl acetate, cis 5, trans 7 - dodecadienoate, cis-5-dodecenol and cis-5-dodecenyl acetate with a chemical purity of 95% and a stereoisomeric purity of 91%. Weigh cis 5, trans 7-dodecadienyl acetate 3 mg / each lure, cis 5, trans 7-dodecadienol 2.9 mg / each lure and cis 5, trans 7-deca Dicarbadiacrylate 1.2mg / each lure, cis-5-dodecenyl acetate 0.2mg / each lure and cis-5-dodecenol 0.3mg / each lure, the five The ingredients are mixed uniformly to make a sex attractant. Then get the cuff type compound rubber stopper carrier that buys on the market, this compound rubber contains the chlorinated butyl rubber of 30~70% (W / W) and the natural rubber of 70~30%; The sex attractant that will make is dissolved in In n-hexane, the concentration is 100 μg / μl, dropwise added to the composite rubber stopper (the amount of 5 components in each rub...
Embodiment 2
[0087]This embodiment makes sex pheromone attractant lure core, adopts cis 5, trans 7-dodecadienol, cis 5, trans 7-dodecadienyl acetate, cis 5, trans 7 - Dodecadienoate, cis-5-dodecenol and cis-5-dodecenyl acetate with a chemical purity of 95% and a stereoisomeric purity of 91%. Weigh cis 5, trans 7-dodecadienyl acetate 2 mg / each lure, cis 5, trans 7-dodecadienol 2 mg / each lure, cis 5, trans 7- Dodecadiacrylate 0.7mg / each lure, cis-5-dodecenyl acetate 0.5mg / each lure and cis-5-dodecenol 0.5mg / each lure, will The five ingredients are mixed evenly to make a sex attractant. Then take the cuff-type composite rubber stopper purchased on the market as a carrier, use the prepared sex attractant, and add 100 μL dropwise to the septum of the cuff-type composite rubber stopper (the dripping amount of 5 components on each compound rubber stopper septum) 2mg: 2mg: 0.7mg: 0.5mg: 0.5mg); then add antioxidants to the prepared lures, take 20 μL of butyl hydroxyanisole or 2,6-di-tert-butyl p...
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