Reducing agent used for producing industrial silicon
A technology of reducing agent and industrial silicon, applied in the direction of silicon compounds, inorganic chemistry, non-metallic elements, etc., can solve the problem of no substantial breakthrough in process formula and reducing agent
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Embodiment 1
[0023] 1) Mix 40kg of washed coal, 30kg of high-purity carbon powder and 30kg of petroleum coke uniformly to obtain a mixture, and pulverize the particle size of the mixture to below 200 mesh, wherein the washed coal contains 8% by mass of ash and 65% by mass of fixed carbon, high-purity Charcoal powder contains 8% by mass of ash and 80% by mass of fixed carbon, and petroleum coke contains 5% by mass of ash and 90% by mass of fixed carbon;
[0024] 2) Add 8kg of coal tar as a binder, stir evenly, granulate, and dry at 200°C for 15 minutes;
[0025] 3) Sieve, and take the cohesive product with a particle size of 10-30mm to obtain silica coke.
[0026] The performance comparison of gained silica coke and charcoal is described in the following table:
[0027] indicators
[0028] Compared with charcoal, the mass % of ash in silicon coke is reduced from 5% to 3.6%. The reduction of ash can increase the content of fixed carbon, and at the same time reduce unnecessary oxid...
Embodiment 2
[0030] 1) Mix 50kg of water-washed coal, 20kg of high-purity carbon powder and 30kg of petroleum coke to obtain a mixture, and crush the mixture to a particle size below 200 mesh, wherein the water-washed coal contains 8% by mass of ash and 65% by mass of fixed carbon, high-purity The charcoal powder contains 8% by mass of ash and 80% by mass of fixed carbon, and the petroleum coke contains 5% by mass of ash and more than 90% by mass of fixed carbon;
[0031] 2) Add 10kg of binder, stir evenly, granulate, and dry at 200°C for 15 minutes;
[0032] 3) Sieve, and take the cohesive product with a particle size of 10-30mm to obtain silica coke.
[0033] The performance comparison of gained silica coke and charcoal is described in the following table:
[0034] indicators
[0035] Compared with charcoal, the mass% of solid carbon in silicon coke increased from 72% to 92.1%, the mass% of ash content decreased from 5% to 3.9%, the structural strength and specific resistance ...
Embodiment 3
[0037] 1) Mix 30kg of washed coal, 30kg of high-purity carbon powder and 40kg of petroleum coke uniformly to obtain a mixture, and pulverize the particle size of the mixture to below 200 mesh, wherein the washed coal contains 8% by mass of ash and 65% by mass of fixed carbon, high-purity The charcoal powder contains 8% by mass of ash and 80% by mass of fixed carbon, and the petroleum coke contains 5% by mass of ash and more than 90% by mass of fixed carbon;
[0038] 2) Add 15kg of binder, stir evenly, granulate, and dry at 200°C for 15 minutes;
[0039] 3) Sieve, and take the cohesive product with a particle size of 10-30mm to obtain silica coke.
[0040] The performance comparison of gained silica coke and charcoal is described in the following table:
[0041] indicators
[0042] Volatile matter, %
[0043] Compared with charcoal, the mass% of solid carbon in silicon coke increased from 72% to 94.1%, the mass% of ash content decreased from 5% to 1.9%, the...
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