Extracting method for radix ophiopogonis extract and dark plum extract as well as cigarette containing radix ophiopogonis extract and dark plum extract
An extraction method and technology of Ophiopogon ebony, applied in the directions of tobacco, tobacco processing, application, etc., can solve the problems of inability to meet the various needs of consumers, and achieve the effects of enhancing the sense of rejuvenation, improving the quality of cigarettes, and comforting the throat
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Embodiment 1
[0038] Example 1, take hot water to extract Ophiopogon japonicus ebony extract, wherein the mass percentage is 50% of Ophiopogon japonicus ebony, and 50% of Ophiopogon japonicus is dissolved in 50% ethanol and added to cigarette shreds. The volume concentration of Ophiopogon japonicus ebony extract solution is 10% %, the amount of Ophiopogon ebony extract is 1% of the mass of shredded tobacco to make cigarettes. When smoked by Guangdong provincial cigarette smokers, the cigarette smoke is full-bodied, full-bodied, and has no peculiar smell. / T 254-2008 High Performance Liquid Chromatography for the Determination of Main Carbonyl Compounds in Cigarette Mainstream Smoke, the detection of smoke has a harmful effect, and the test results are shown in Table 1.
Embodiment 2
[0039] Example 2, according to the mass percentage, 75% of ebony plum and 25% of Ophiopogon japonicus, take dried Ophiopogon japonicus and ebony plum, remove impurities, dry at 60°C, and pulverize to 10-100 mesh, add 90°C hot water according to the mass ratio of 1:10 , leaching at 90°C, once for 5 hours, leaching twice, combining the two water extracts, filtering, and decompressing and concentrating the filtrate under the conditions of 0.05Mpa, 60°C, and 2 hours, and the concentrated filtrate Add 5 times the volume of 75% ethanol, let stand at no more than 4°C for 12 hours, centrifuge at 4000 rpm, and filter to obtain Ophiopogon ebony extract. The Ophiopogon ebony extract is dissolved in 10% ethanol and then added to cigarette shreds, the solution volume concentration of the Ophiopogon ebony extract is 10%, and the dosage of the Ophiopogon ebony extract is 0.1% of the mass of the cut tobacco. When smoked by Guangdong Provincial Cigarette Testers, the cigarette smoke is full-bo...
Embodiment 3
[0040] Example 3, according to the mass percentage of ebony 40%, Ophiopogon japonicus 60%, will take dried Ophiopogon japonicus and ebony plum, remove impurities, dry at 60°C, extract with 20°C water for 2 hours, the mass ratio of solid to liquid is 1:15, Ultrasonic power is 80W / cm 2 , the treatment time is 30 minutes, filter, the filtrate is decompressed and concentrated under the conditions of 0.05Mpa, 60°C, and 2 hours, add 10 times the volume of 75% ethanol to the concentrated filtrate, and let it stand for 12 hours at no more than 10°C, centrifuge The rotating speed is 4000 rpm, filtered to obtain Ophiopogon ebony extract. The Ophiopogon ebony extract is dissolved in 75% ethanol and then added to shredded tobacco. The solution volume concentration of the Ophiopogon ebony extract is 8%, and the dosage of the Ophiopogon ebony extract is 0.01% of the weight of the shredded tobacco. When smoked by Guangdong Provincial Cigarette Testers, the smoke of cigarettes is mellow and ...
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