Technological method for extracting caffeine and tea polyphenol mixture from tea step by step
A process method and technology for caffeine, which are applied in the field of step-by-step extraction of caffeine and tea polyphenol mixture, can solve the problems of difficult large-scale production, cumbersome process, low yield and the like, and achieve a low extraction temperature, simple process and high extraction rate. Effect
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Embodiment 1
[0025] The steps and conditions of a process method for extracting a mixture of caffeine and tea polyphenols step by step from tea leaves are as follows:
[0026] Step 1: Extract caffeine
[0027] (1) After crushing 250 grams of dried tea leaves to 20 mesh, place them in 1 liter of supercritical CO 2 in the extraction kettle, and then turn on the CO 2 The high-pressure pump injects high-pressure CO into the extraction kettle at a flow rate of 3L / h 2 At the same time, open the entrainer pump and inject the entrainer that is water in the ratio of 1:0.1 according to the solid-liquid ratio into the extraction kettle;
[0028] (2) When the pressure in the extraction kettle rises to 20MPa, and the pressure is kept constant by adjusting the valve between the extraction kettle and the analysis kettle, the high-pressure CO containing the extract caffeine and the entrainer 2 The gas enters the desorption tank that has been kept at 40°C, and the CO in the desorption tank 2 After gas ...
Embodiment 2
[0034] The steps and conditions of a process method for extracting a mixture of caffeine and tea polyphenols step by step from tea leaves are as follows:
[0035] Step 1: Extract caffeine
[0036] (1) After crushing 250 grams of dried tea leaves to 30 mesh, place them in 1 liter of supercritical CO 2 in the extraction kettle, and then turn on the CO 2 The high-pressure pump injects high-pressure CO into the extraction kettle at a flow rate of 4L / h 2 gas, and simultaneously open the entrainer pump and inject the entrainer, i.e. 30% ethanol, into the extraction kettle by solid-liquid ratio of 1:0.5;
[0037] (2) When the pressure in the extraction kettle rises to 24MPa, and the pressure is kept constant by adjusting the valve between the extraction kettle and the analysis kettle, the high-pressure CO containing the extract caffeine and the entrainer 2 The gas enters the desorption tank that has been kept at 48°C, and the CO in the desorption tank 2 After separation of the ga...
Embodiment 3
[0043] The steps and conditions of a process method for extracting a mixture of caffeine and tea polyphenols step by step from tea leaves are as follows:
[0044] Step 1: Extract caffeine
[0045] (1) After crushing 250 grams of dried tea leaves to 40 mesh, place them in 1 liter of supercritical CO 2 in the extraction kettle, and then turn on the CO 2The high-pressure pump injects high-pressure CO into the extraction kettle at a flow rate of 5L / h 2 At the same time, open the entrainer pump and inject the entrainer that is water in the ratio of 1:0.6 according to the solid-liquid ratio into the extraction kettle;
[0046] (2) When the pressure in the extraction kettle rises to 28MPa, and the pressure is kept constant by adjusting the valve between the extraction kettle and the analysis kettle, the high-pressure CO containing the extract caffeine and the entrainer 2 The gas enters the desorption tank that has been kept at 55°C, and the CO in the desorption tank 2 After gas i...
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