C.i. pigment red 112 with improved dispersion
A pigment red, dispersing technology, applied in organic dyes, azo dyes, household appliances, etc., can solve problems such as performance impact
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Embodiment 1
[0046] 1.1) Preparation of the diazonium salt solution of 2,4,5-trichloroaniline:
[0047] 250 parts of water were previously added and at room temperature first 40.3 parts of 2,4,5-trichloroaniline were added with stirring and admixed with 193 parts by volume of 31% strength hydrochloric acid. It was then cooled to 0°C with ice. The diazotization was carried out with 29 parts by volume of a 40% strength sodium nitrite solution. The diazonium salt solution formed is filtered off into a receiving vessel after addition of a clarification aid. Excess nitrite was removed by adding sulfamic acid and the temperature was maintained at 10°C by external cooling.
[0048] 1.2) Preparation of a solution of the coupling component (naphthol):
[0049] At room temperature, 190 parts of water and 28 parts by volume of 33% sodium hydroxide solution, and 1 part of alkylsulfonate were pre-added, and 60 parts of N-(2-methylphenyl)-2-hydroxy-3 - Naphthamide. The mixture was stirred until a c...
Embodiment 2
[0057] The synthesis was carried out as described in Example 1, where step 1.3) was followed by grinding the precipitated coupler via a Dispax mill. The dispersion hardness is 25, the residual coupler content is 0.69%, and the polychlorinated biphenyl content is 3ppm.
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