Platinum black pulse plating method based on ultrasonic assistance
A pulsed electroplating, ultrasonic-assisted technology, applied in the field of ultrasonic-assisted platinum black pulse electroplating, can solve the problems of poor adhesion between the coating and the substrate, large diameter of platinum black particles, easy to fall off, etc., to achieve increased charge storage, AC impedance Reduced, good binding effect
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Embodiment 1
[0019] Such as figure 1 As shown, this embodiment was prepared through the following steps:
[0020] The first step is to clean the platinum electrode and platinum wire auxiliary electrode;
[0021] The cleaning refers to ultrasonic cleaning.
[0022] Step 2: Put the platinum electrode to be electroplated and the platinum wire auxiliary electrode into the electroplating solution vertically, and connect the negative and positive electrodes of the power supply respectively;
[0023] The diameter of the platinum electrode to be electroplated is 60 μm, and the electrode spot width is 60 μm.
[0024] The electroplating solution refers to a solution obtained by dissolving 3 grams of chloroplatinic acid and 0.01 grams of lead acetate in 100 grams of water.
[0025] Step 3: Put the electroplating tank containing the electroplating solution into the ultrasonic generator, turn on the ultrasonic generator and apply pulse current;
[0026] The pulse current refers to a duty cycle of 5μs: 500μs and a ...
Embodiment 2
[0030] Such as figure 2 As shown, this embodiment was prepared through the following steps:
[0031] The first step is to clean the platinum electrode and platinum wire counter electrode to be electroplated;
[0032] The cleaning refers to ultrasonic cleaning.
[0033] Step 2: Put the platinum electrode to be electroplated and the platinum wire auxiliary electrode into the electroplating solution vertically, and connect the negative and positive electrodes of the power supply respectively;
[0034] The diameter of the platinum electrode to be electroplated is 200 μm, and the electrode spot width is 200 μm.
[0035] The electroplating solution refers to a solution obtained by dissolving 3 grams of chloroplatinic acid and 0.01 grams of lead acetate in 100 grams of water.
[0036] Step 3: Put the electroplating tank containing the electroplating solution into the ultrasonic generator, turn on the ultrasonic generator and apply pulse current;
[0037] The pulse current refers to a duty ratio...
Embodiment 3
[0041] Such as image 3 As shown, this embodiment was prepared through the following steps:
[0042] The first step is to clean the platinum electrode and platinum wire auxiliary electrode;
[0043] The cleaning refers to ultrasonic cleaning.
[0044] Step 2: Put the platinum electrode to be electroplated and the platinum wire auxiliary electrode into the electroplating solution vertically, and connect the negative and positive electrodes of the power supply respectively;
[0045] The diameter of the platinum electrode to be electroplated is 400 μm, and the electrode spot width is 400 μm.
[0046] The electroplating solution refers to a solution obtained by dissolving 3 grams of chloroplatinic acid and 0.01 grams of lead acetate in 100 grams of water.
[0047] Step 3: Put the electroplating tank containing the electroplating solution into the ultrasonic generator, turn on the ultrasonic generator and apply pulse current;
[0048] The pulse current refers to a duty cycle of 5μs: 500μs and...
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