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Quasicrystal particle reinforced magnesium matrix composite material and preparation method thereof

A composite material and particle reinforcement technology, which is applied in the field of quasicrystal particle reinforced magnesium-based composite material and its preparation, Mg-Zn-Gd based thermally stable icosahedral quasicrystal-reinforced magnesium-based composite material, which can solve the problem of quasicrystal content Difficult to control, difficult to disperse evenly, high energy consumption, etc., to avoid different expansion coefficients, poor wettability, and simple processing procedures

Inactive Publication Date: 2010-07-28
BEIJING UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In the Chinese patent ZL00111624.X "Quasicrystal Reinforced Magnesium Matrix Composite Material", Xu Zhou from Shanghai Jiaotong University prepared the AlCuFe quasicrystal reinforced magnesium matrix composite material by stirring casting method, the highest tensile strength is 155.6MPa, and the elongation The highest is 4.1%. It should be said that the magnesium-based composite material prepared by this invention is not enough to meet the demand under the current application conditions; Guo Xuefeng et al. in the Chinese patent (ZL03134363. Quasicrystalline phase reinforced magnesium alloy, and the quasicrystalline content is not easy to control and it is difficult to disperse uniformly, the process is more complicated, the energy consumption is large, it is not a recycled material, and the cost is high

Method used

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  • Quasicrystal particle reinforced magnesium matrix composite material and preparation method thereof
  • Quasicrystal particle reinforced magnesium matrix composite material and preparation method thereof
  • Quasicrystal particle reinforced magnesium matrix composite material and preparation method thereof

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Experimental program
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Effect test

Embodiment 1

[0018] Get 38 grams of pure Mg particles, 2 grams of quasicrystal particles Mg-Zn-Gd, that is, the weight ratio of the quasicrystal particle addition is 5%, and prepare as follows:

[0019] I. Prepare quasi-crystalline particles by ball milling, with a particle size of 20-100um;

[0020] II. Mix quasicrystalline particles and magnesium powder into the repeated plastic deformation equipment, and the number of deformations is selected to be 100 times;

[0021] III. The magnesium-based composite material obtained by repeated plastic deformation is extruded in a reverse extrusion die of 1:10, the extrusion temperature is 300 ° C, and the extrusion rate is 6 mm / min;

[0022] Tensile strength of the prepared composite profile: 268MPa; elongation after fracture: 9.7%

Embodiment 2

[0024] Get 36 grams of pure Mg particles, 4 grams of quasicrystal particles Mg-Zn-Gd, that is, the weight ratio of the quasicrystal particle addition is 10%, and it is prepared as follows:

[0025] I. Prepare quasi-crystalline particles by ball milling, with a particle size of 20-100um;

[0026] II. Mix quasicrystalline particles and magnesium powder into repeated plastic deformation equipment, and select 200 times of deformation times;

[0027] III. The magnesium-based composite material obtained by repeated plastic deformation is extruded in a reverse extrusion die of 1:16, the extrusion temperature is 360 ° C, and the extrusion rate is 6mm / min;

[0028] Tensile strength of the prepared composite profile: 309MPa; elongation after fracture: 7.0%

Embodiment 3

[0030] Get 34 grams of pure Mg particles, 6 grams of quasicrystal particles Mg-Zn-Gd, that is, the weight ratio of the quasicrystal particle addition is 15%, prepared as follows:

[0031] I. Prepare quasicrystalline particles by ball milling, with a size of 20-100um;

[0032] II. Mix quasicrystalline particles and magnesium powder into repeated plastic deformation equipment, and select 200 times of deformation times;

[0033] III. The magnesium-based composite material obtained by repeated plastic deformation is extruded in a reverse extrusion die of 1:25, the extrusion temperature is 320 ° C, and the extrusion rate is 6 mm / min;

[0034] Tensile strength of the prepared composite profile: 292MPa; elongation after fracture: 5.4%

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Abstract

The invention discloses a quasicrystal particle reinforced magnesium matrix composite material and a preparation method thereof. The composite material matrix is industrial pure magnesium; the reinforced particle is Mg-Zn-Gd quasicrystal particle, the size of the quasicrystal particle is of 20-100um, and the weight percentage of the quasicrystal particle is of 5-30 percent. The preparation method is as follows: by adopting the repeated plastic deformation technology processing procedure, the proportion of the quasicrystal particles is accurately controlled according to different purposes of the magnesium matrix material, so as to achieve the optimal combination of the intensity and elongation and lead the prepared composite material to meet different needs.

Description

technical field [0001] The invention relates to a magnesium-based composite material reinforced by quasi-crystal particles and a preparation method thereof, in particular to a Mg-Zn-Gd-based thermally stable icosahedral quasi-crystal-reinforced magnesium-based composite material prepared by repeated plastic deformation, which belongs to the composite Materials and light alloy processing field. Background technique [0002] Since the early 1990s, the application and development trend of major metal materials in the world has changed significantly. With the increasing awareness of environmental protection and energy saving, material researchers and product designers pay more and more attention to issues such as product lightweight and recyclability. As the lightest engineering metal material at present, magnesium alloy has become a representative of light metal materials due to its high specific strength and recyclability, and it has continued to grow at a rate of 20% per yea...

Claims

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Application Information

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IPC IPC(8): C22C23/04C22C1/04C22F1/06
Inventor 杜文博王旭东王朝辉李淑波
Owner BEIJING UNIV OF TECH
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