Method for purifying and reclaiming carbon dioxide from landfill gas and device thereof
A landfill gas and carbon dioxide technology, applied in chemical instruments and methods, separation methods, liquefaction, etc., can solve problems affecting the environment, waste of resources, complex composition of landfill gas, etc., achieve a wide range of applications and avoid environmental pollution Effect
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Embodiment 1
[0063] After desulfurization, deoxidation, compression and other pretreatment steps, the feed gas enters the first-stage pressure swing adsorption unit, the adsorption pressure is 0.3MPa, the adsorption time is 100s, and then the gas containing 91% CH 4 The adsorbed gas is collected from the top of the tower; the pressure in the tower is equalized, reversed, and reduced to normal pressure, and the CO in the desorbed gas obtained from the bottom of the tower 2 The content is 70%, the remainder is N2, O2 and CH 4 ; The desorbed gas enters the two-stage PSA unit, the operating conditions are the same as that of the program, the adsorbed gas is discharged from the top of the tower, and the CO in the desorbed gas discharged from the bottom of the tower is 2 Increase to 91%, continue to use rectification for purification, and finally obtain food-grade liquid CO with a purity of 99.993% 2 .
Embodiment 2
[0065] After desulfurization, deoxidation, compression and other pretreatment steps, the feed gas enters the primary pressure swing adsorption unit, the adsorption pressure is 1.2MPa, the adsorption time is 280s, and then the gas containing 93% CH 4 The adsorbed gas is collected from the top of the tower; the pressure in the tower is equalized, reversed, and reduced to normal pressure, and the CO in the desorbed gas obtained from the bottom of the tower 2 The content is 73%, the remainder is N2, O2 and CH 4 ; The desorbed gas enters the two-stage PSA unit, the operating conditions are the same as that of the program, the adsorbed gas is discharged from the top of the tower, and the CO in the desorbed gas discharged from the bottom of the tower is 2 Increase to 92%, continue to use rectification for purification, and finally obtain food-grade liquid CO with a purity of 99.996% 2 .
Embodiment 3
[0067] After desulfurization, deoxidation, compression and other pretreatment steps, the feed gas enters the primary pressure swing adsorption unit, the adsorption pressure is 2.0MPa, the adsorption time is 300s, and then the gas containing 95% CH 4 The adsorbed gas is collected from the top of the tower; the pressure in the tower is equalized, reversed, and reduced to normal pressure, and the CO in the desorbed gas obtained from the bottom of the tower 2 The content is 77%, the remainder is N2, O2 and CH 4 ; The desorbed gas enters the two-stage PSA unit, the operating conditions are the same as that of the program, the adsorbed gas is discharged from the top of the tower, and the CO in the desorbed gas discharged from the bottom of the tower is 2 Increase to 93%, continue to use rectification for purification, and finally obtain food-grade liquid CO with a purity of 99.999% 2.
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