Preparation method of high efficient rare-earth paint drier
A drier and rare earth technology, applied in the field of preparation of high-efficiency rare earth element paint drier, can solve the problems of environmental pollution, expensive cobalt soap, poisonous lead soap, etc.
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Embodiment 1
[0013] Add 15L of 200# solvent oil to 5L of 6.0mol / L isooctanoic acid, mix under stirring for 10 minutes, add 6.0L of prepared sodium hydroxide solution with a concentration of 4.0mol / L to carry out saponification reaction, and the time is 30 minutes After saponification, add 10L of lanthanum and cerium solution to the solution for extraction reaction, the reaction time is 40 minutes, then add 1.2L of drying aid to the solution, and perform extraction reaction for 60 minutes, then transfer the solution into a separatory funnel Stand in the medium for 4 hours to separate the layers, and the separated organic phase is the product of isooctanoic acid rare earth drier. Its metal content is 6.18%, clear and transparent oily liquid.
Embodiment 2
[0015] Add 30L of 200# solvent oil to 10L of 6.0mol / L isooctanoic acid, stir and mix for 10 minutes, then add 8.0L of prepared sodium hydroxide solution with a concentration of 6.0mol / L to carry out saponification reaction for 30 minutes After saponification, add 20L of lanthanum and cerium solution to the solution for extraction reaction, the reaction time is 40 minutes, then add 1.52L of drying aid to the solution for extraction reaction, time is 40 minutes, then transfer the solution to a separatory funnel for static Set for 6 hours to separate the layers, and the separated organic phase is the product of isooctanoic acid rare earth drier. Its metal content is 6.5%, clear and transparent oily liquid.
Embodiment 3
[0017] Add 90L 200# solvent oil to 30L concentration of 6.0mol / L isooctanoic acid, stir and mix for 10 minutes, add 24L of sodium hydroxide solution with a concentration of 6.0mol / L to carry out saponification reaction, the time is 30 minutes, saponification After the end, add 20L of lanthanum and cerium solution to the solution for the extraction reaction, the reaction time is 60 minutes, then add 7.36L of drying aid to the solution for the extraction reaction, the time is 60 minutes, then transfer the solution to the separatory funnel and let it stand for 5 minutes. After hours of stratification, the separated organic phase is the product of isooctanoic acid rare earth drier. Its metal content is 6.20%, clear and transparent oily liquid.
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