Unsubstituted and polymeric leuco colorants for coloring consumer products
A technology of colorants and polymers, applied in dyeing methods, textiles and papermaking, washing composition dyes, etc., can solve problems such as undisclosed leuco colorants
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[0076] The following examples are provided to further describe the unsubstituted polymeric leuco colorants of the present invention; however, they should not be construed to limit the invention as defined in the appended claims. In fact, it will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the scope or spirit of the invention. All parts and percentages given in these examples are by weight unless otherwise indicated.
[0077] Sample Preparation
[0078] General Step 1: For Nitrile Addition to TPM
[0079] Colorants 1-12 and 26 of Tables 1 and 2 were made, for example, using the following general procedure.
[0080] A 500 mL four-necked round bottom flask was equipped with a thermocouple, heating mantle, mechanical stirrer, and inlet and outlet ports connected to an air scrubber bath containing 10% NaOH solution. The polymerized triphenylmethane (0.080 mol) was poured into the f...
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