Method for monitoring heavy metal pollution of urban roads
A pollution monitoring and heavy metal technology, which is applied in the preparation of test samples, thermal excitation analysis, sampling devices, etc., can solve the problems that are rarely reported in research, and achieve the effect of protecting the environment and maintaining ecological balance
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Embodiment 1
[0018] (1) Select representative road intersections as sampling points, including overpasses with a lot of traffic flow within the inner ring. Collect dust samples from the ground. The collected dust samples are air-dried naturally. Use a finer sieve to sieve the finer dust part to remove sand, plant debris and other impurities in the sample, and set aside;
[0019] (2) Accurately weigh 0.5000g of soil sample, add 1.5ml H 2 SO 4 , 3ml HNO 3 , 9ml HCl, heated at a constant temperature of 160°C, until there is little brown gas, add 0.5ml HClO 4 Digest until the solution is clear and the precipitate is white; raise the temperature slightly to catch HClO 4 , the solution was evaporated to near dryness;
[0020] (3) Add 0.5ml HNO to the digested sample 3 , add a little deionized water to dissolve, then transfer to a 10ML colorimetric tube, dilute to volume with deionized water, and store;
[0021] (4) Take the upper clear night, and use CP-AES to measure the Cr, Mn, Ni, Cu, Z...
Embodiment 2
[0022] Embodiment 2 (more detailed experimental process is as follows)
[0023] sampling
[0024]The sampling method refers to the "Collection and Processing of Soil Samples", and according to the distribution of roads in Tianjin, select representative road intersections as sampling points, including within the inner ring, between the inner and middle rings, and between the middle and outer rings. Main arterial roads and secondary arterial roads with relatively less traffic volume, and overpass bridges with more traffic volume. Collect ground dust samples and bring them back to the laboratory. The plow layer soil was collected as a control to evaluate the heavy metal pollution in road dust.
[0025] Sample pretreatment
[0026] Air-dry the collected dust samples naturally, and use a finer sieve to sieve the finer dust part to remove sand, plant debris and other impurities in the sample, so that the experiment can avoid the interference of irrelevant impurities and make the ...
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